(<(tetrahydro-3'',4'',5'',6''-2''H-pyranyl-2'')oxy>-4'-butyl)-3-tetratosyl-1,5,9,13-tetraaza-1,5,9,13-cyclohexadecane

Base Information

Chemical Name:(<(tetrahydro-3'',4'',5'',6''-2''H-pyranyl-2'')oxy>-4'-butyl)-3-tetratosyl-1,5,9,13-tetraaza-1,5,9,13-cyclohexadecane
CAS No.:118467-57-5
Molecular Formula:C₄₉H₆₈N₄O₁₀S₄
Molecular Weight:1001.36
Hs Code.:

Synonyms:(<(tetrahydro-3'',4'',5'',6''-2''H-pyranyl-2'')oxy>-4'-butyl)-3-tetratosyl-1,5,9,13-tetraaza-1,5,9,13-cyclohexadecane

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Chemical Property of (<(tetrahydro-3'',4'',5'',6''-2''H-pyranyl-2'')oxy>-4'-butyl)-3-tetratosyl-1,5,9,13-tetraaza-1,5,9,13-cyclohexadecane

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Technology Process of (<(tetrahydro-3'',4'',5'',6''-2''H-pyranyl-2'')oxy>-4'-butyl)-3-tetratosyl-1,5,9,13-tetraaza-1,5,9,13-cyclohexadecane

There total 1 articles about (<(tetrahydro-3'',4'',5'',6''-2''H-pyranyl-2'')oxy>-4'-butyl)-3-tetratosyl-1,5,9,13-tetraaza-1,5,9,13-cyclohexadecane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 67341-38-2
N,N'-bis<3-(tosylamino)propyl>-N,N'-ditosyl-1,3-propanediamine

: 118481-88-2
2-<4-(tetrahydropyran-2-yloxy)butyl>propane-1,3-diol di-p-toluenesulfonate

: 118467-57-5
(<(tetrahydro-3'',4'',5'',6''-2''H-pyranyl-2'')oxy>-4'-butyl)-3-tetratosyl-1,5,9,13-tetraaza-1,5,9,13-cyclohexadecane

Guidance literature:: With sodium hydride; In N,N-dimethyl-formamide; for 2h;
DOI:10.1002/hlca.19880710313

Reference yield:

: 118467-57-5
(<(tetrahydro-3'',4'',5'',6''-2''H-pyranyl-2'')oxy>-4'-butyl)-3-tetratosyl-1,5,9,13-tetraaza-1,5,9,13-cyclohexadecane

: 118467-60-0
(tetratosyl-1',5',9',13'-tetraaza-1',5',9',13'-cyclohexadecyl-3')-4-butanol

Guidance literature:: With toluene-4-sulfonic acid; In 1,4-dioxane; for 2h; Yield given; Ambient temperature;
DOI:10.1002/hlca.19880710313

Reference yield:

: 118467-57-5
(<(tetrahydro-3'',4'',5'',6''-2''H-pyranyl-2'')oxy>-4'-butyl)-3-tetratosyl-1,5,9,13-tetraaza-1,5,9,13-cyclohexadecane

: 118467-66-6
(tetratosyl-1',5',9',13'-tetraaza-1',5',9',13'-cyclohexadecyl-3')-5-pentanenitrile

Guidance literature:: Multi-step reaction with 3 steps

1: TsOH / dioxane / 2 h / Ambient temperature

2: 80 percent / pyridine / 3.5 h / 0 °C

3: 70 percent / dimethylsulfoxide / 2 h / 95 °C

With toluene-4-sulfonic acid; In 1,4-dioxane; pyridine; dimethyl sulfoxide;
DOI:10.1002/hlca.19880710313