Technology Process of C15H16O3
There total 5 articles about C15H16O3 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 5 steps
1: toluene-4-sulfonic acid / 70 °C
2: triethylamine; magnesium chloride / 80 °C
3: potassium carbonate; sodium iodide / N,N-dimethyl-formamide / 60 °C
4: diphenyl diselenide; dihydrogen peroxide / dichloromethane / 48 h / 20 °C
5: methanol; ammonia / 96 h
With
methanol; diphenyl diselenide; ammonia; dihydrogen peroxide; potassium carbonate; toluene-4-sulfonic acid; triethylamine; sodium iodide; magnesium chloride;
In
dichloromethane; N,N-dimethyl-formamide;
4: Baeyer-Villiger oxidation;
DOI:10.1016/j.tetlet.2011.07.063
- Guidance literature:
-
Multi-step reaction with 2 steps
1: diphenyl diselenide; dihydrogen peroxide / dichloromethane / 48 h / 20 °C
2: methanol; ammonia / 96 h
With
methanol; diphenyl diselenide; ammonia; dihydrogen peroxide;
In
dichloromethane;
1: Baeyer-Villiger oxidation;
DOI:10.1016/j.tetlet.2011.07.063