C₁₅H₁₆O₃

Base Information

• Chemical Name: C₁₅H₁₆O₃
• CAS No.: 1333081-72-3
• Molecular Formula: C₁₅H₁₆O₃
• Molecular Weight: 244.29
• Mol file: 1333081-72-3.mol

Synonyms:C₁₅H₁₆O₃

Chemical Property of C₁₅H₁₆O₃

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₁₅H₁₆O₃

There total 5 articles about C₁₅H₁₆O₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

C18H18O5 (1333081-69-8) → C15H16O3 (1333081-72-3)

Guidance literature:

With methanol; ammonia; for 96h;

DOI:10.1016/j.tetlet.2011.07.063

Reference yield:

p-hydroxyphenethyl alcohol (501-94-0) → C15H16O3 (1333081-72-3)

Guidance literature:

Multi-step reaction with 5 steps

1: toluene-4-sulfonic acid / 70 °C

2: triethylamine; magnesium chloride / 80 °C

3: potassium carbonate; sodium iodide / N,N-dimethyl-formamide / 60 °C

4: diphenyl diselenide; dihydrogen peroxide / dichloromethane / 48 h / 20 °C

5: methanol; ammonia / 96 h

With methanol; diphenyl diselenide; ammonia; dihydrogen peroxide; potassium carbonate; toluene-4-sulfonic acid; triethylamine; sodium iodide; magnesium chloride; In dichloromethane; N,N-dimethyl-formamide; 4: Baeyer-Villiger oxidation;

DOI:10.1016/j.tetlet.2011.07.063

Reference yield:

4-(benzyloxy)-3-formyl phenethyl acetate (1237517-66-6) → C15H16O3 (1333081-72-3)

Guidance literature:

Multi-step reaction with 2 steps

1: diphenyl diselenide; dihydrogen peroxide / dichloromethane / 48 h / 20 °C

2: methanol; ammonia / 96 h

With methanol; diphenyl diselenide; ammonia; dihydrogen peroxide; In dichloromethane; 1: Baeyer-Villiger oxidation;

DOI:10.1016/j.tetlet.2011.07.063

upstream raw materials:

4-(benzyloxy)-3-formyl phenethyl acetate

C₁₈H₁₈O₅

p-hydroxyphenethyl alcohol

2-(4-hydroxyphenyl)ethyl acetate