3-phenylpropynal oxime

Base Information

• Chemical Name: 3-phenylpropynal oxime
• CAS No.: 858445-43-9
• Molecular Formula: C₉H₇NO
• Molecular Weight: 145.161
• Mol file: 858445-43-9.mol

Synonyms:3-phenylpropynal oxime

Chemical Property of 3-phenylpropynal oxime

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

Useful:

Technology Process of 3-phenylpropynal oxime

There total 5 articles about 3-phenylpropynal oxime which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

Phenylpropargyl aldehyde (2579-22-8) → 3-phenylpropynal oxime (858445-43-9)

Guidance literature:

With hydroxylamine hydrochloride; In dimethyl sulfoxide; at 90 ℃;

DOI:10.1055/s-0030-1261181

Reference yield:

Phenylpropargyl aldehyde (2579-22-8) → 3-phenylpropynal oxime (858445-43-9) + (E)-3-phenylpropyl-2-yn-1-one oxime

Guidance literature:

With hydroxylamine hydrochloride; sodium hydrogencarbonate; In methanol; Title compound not separated from byproducts.;

DOI:10.1134/S1070428007110243

Reference yield:

→ 3-phenylpropynal oxime (858445-43-9)

Guidance literature:

With sodium hydroxide;

upstream raw materials:

α-bromo-cis-cinnamaldehyde seqtrans-oxime

Phenylpropargyl aldehyde

Downstream raw materials:

3-Phenyl-2-propynonitrile

tert-butyl 3-(phenylethynyl)-1-oxa-2,8-diazaspiro[4.5]dec-2-ene-8-carboxylate

3-phenylethynyl-1-oxa-2,8-diazaspiro[4.5]dec-2-ene

3-phenylethynyl-8-(6-methyl-3-nitro-2-pyridyl)-1-oxa-2,8-diazaspiro[4.5]dec-2-ene