N-benzyl-1-methyl-N-[2-[N-(trityloxy)ethanimidoyl]phenyl]-2,5-cyclohexadiene-1-carboxamide

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Chemical Name:N-benzyl-1-methyl-N-[2-[N-(trityloxy)ethanimidoyl]phenyl]-2,5-cyclohexadiene-1-carboxamide
CAS No.:766512-24-7
Molecular Formula:C₄₂H₃₈N₂O₂
Molecular Weight:602.776
Hs Code.:

Synonyms:N-benzyl-1-methyl-N-[2-[N-(trityloxy)ethanimidoyl]phenyl]-2,5-cyclohexadiene-1-carboxamide

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Chemical Property of N-benzyl-1-methyl-N-[2-[N-(trityloxy)ethanimidoyl]phenyl]-2,5-cyclohexadiene-1-carboxamide

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Technology Process of N-benzyl-1-methyl-N-[2-[N-(trityloxy)ethanimidoyl]phenyl]-2,5-cyclohexadiene-1-carboxamide

There total 8 articles about N-benzyl-1-methyl-N-[2-[N-(trityloxy)ethanimidoyl]phenyl]-2,5-cyclohexadiene-1-carboxamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 1-[2-(benzylamino)phenyl]ethanone O-trityloxime

: 85215-58-3
3-methylcyclohexa-1,4-diene-3-carbonyl chloride

: 766512-24-7
N-benzyl-1-methyl-N-[2-[N-(trityloxy)ethanimidoyl]phenyl]-2,5-cyclohexadiene-1-carboxamide

Guidance literature:: With dmap; In pyridine; dichloromethane; Heating;
DOI:10.1021/jo049617f

Reference yield:

: (2-acetylphenyl)benzylamonium chloride

: 766512-24-7
N-benzyl-1-methyl-N-[2-[N-(trityloxy)ethanimidoyl]phenyl]-2,5-cyclohexadiene-1-carboxamide

Guidance literature:: Multi-step reaction with 2 steps

1: 84 percent / H₂SO₄ / ethanol / 60 °C

2: 82 percent / DMAP / pyridine; CH₂Cl₂ / Heating

With dmap; sulfuric acid; In pyridine; ethanol; dichloromethane;
DOI:10.1021/jo049617f

Reference yield:

: 31938-10-0
2-(trityloxy)isoindoline-1,3-dione

: 766512-24-7
N-benzyl-1-methyl-N-[2-[N-(trityloxy)ethanimidoyl]phenyl]-2,5-cyclohexadiene-1-carboxamide

Guidance literature:: Multi-step reaction with 3 steps

1: 92 percent / hydrazine hydrate / CH₂Cl₂ / 0.5 h

2: 84 percent / H₂SO₄ / ethanol / 60 °C

3: 82 percent / DMAP / pyridine; CH₂Cl₂ / Heating

With dmap; sulfuric acid; hydrazine hydrate; In pyridine; ethanol; dichloromethane;
DOI:10.1021/jo049617f