N-[(1R)-1-phenylpropyl]-N-(5,6,7,8-tetrahydropyrido[4',3':4,5]thieno[2,3-d]pyrimidin-4-yl)amine

Base Information

Chemical Name:N-[(1R)-1-phenylpropyl]-N-(5,6,7,8-tetrahydropyrido[4',3':4,5]thieno[2,3-d]pyrimidin-4-yl)amine
CAS No.:1226548-35-1
Molecular Formula:C₁₈H₂₀N₄S
Molecular Weight:324.45
Hs Code.:

Synonyms:N-[(1R)-1-phenylpropyl]-N-(5,6,7,8-tetrahydropyrido[4',3':4,5]thieno[2,3-d]pyrimidin-4-yl)amine

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Chemical Property of N-[(1R)-1-phenylpropyl]-N-(5,6,7,8-tetrahydropyrido[4',3':4,5]thieno[2,3-d]pyrimidin-4-yl)amine

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Technology Process of N-[(1R)-1-phenylpropyl]-N-(5,6,7,8-tetrahydropyrido[4',3':4,5]thieno[2,3-d]pyrimidin-4-yl)amine

There total 2 articles about N-[(1R)-1-phenylpropyl]-N-(5,6,7,8-tetrahydropyrido[4',3':4,5]thieno[2,3-d]pyrimidin-4-yl)amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 1226548-33-9
tert-butyl 4-[(1R)-1-phenylpropyl]amino-5,6,7,8-tetrahydropyrido[4',3':4,5]thieno[2,3-d]pyrimidine-7-carboxylate

: 1226548-35-1
N-[(1R)-1-phenylpropyl]-N-(5,6,7,8-tetrahydropyrido[4',3':4,5]thieno[2,3-d]pyrimidin-4-yl)amine

Guidance literature:: tert-butyl 4-[(1R)-1-phenylpropyl]amino-5,6,7,8-tetrahydropyrido[4',3':4,5]thieno[2,3-d]pyrimidine-7-carboxylate; With trifluoroacetic acid; In dichloromethane; at 0 - 20 ℃; for 2h; Inert atmosphere;

With sodium hydrogencarbonate; In water; Inert atmosphere;
DOI:10.1021/jm100607r

Reference yield:

: 1226548-35-1
N-[(1R)-1-phenylpropyl]-N-(5,6,7,8-tetrahydropyrido[4',3':4,5]thieno[2,3-d]pyrimidin-4-yl)amine

Guidance literature:

Reference yield:

: 13991-36-1
4-bromocrotonic acid

: 1226548-35-1
N-[(1R)-1-phenylpropyl]-N-(5,6,7,8-tetrahydropyrido[4',3':4,5]thieno[2,3-d]pyrimidin-4-yl)amine

: C₂₂H₂₃BrN₄OS

Guidance literature:: With 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane; at 20 ℃; for 2h; Inert atmosphere;
DOI:10.1021/jm100607r