dimethyl 2-(3-methylbenzylidene)succinate

Base Information

Chemical Name:dimethyl 2-(3-methylbenzylidene)succinate
CAS No.:252929-21-8
Molecular Formula:C₁₄H₁₆O₄
Molecular Weight:248.279
Hs Code.:

Synonyms:dimethyl 2-(3-methylbenzylidene)succinate

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Chemical Property of dimethyl 2-(3-methylbenzylidene)succinate

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Technology Process of dimethyl 2-(3-methylbenzylidene)succinate

There total 3 articles about dimethyl 2-(3-methylbenzylidene)succinate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.7%

: 620-13-3
1-bromomethyl-3-methyl-benzene

: 624-49-7
dimethylfumarate

: 252929-21-8
dimethyl 2-(3-methylbenzylidene)succinate

Guidance literature:: With tributylphosphine; caesium carbonate; In toluene; at 60 ℃; for 48h; Inert atmosphere; Schlenk technique;
DOI:10.1021/acs.orglett.1c01214

Reference yield:

: 620-23-5
m-tolyl aldehyde

: 23055-10-9
1,4-dimethyl but-2-enedioate

: 252929-21-8
dimethyl 2-(3-methylbenzylidene)succinate

: dimethyl 2-(3-methylbenzylidene)succinate

Guidance literature:: With trimethoxysilane; 3-Methyl-1-phenyl-2-phospholene 1-oxide; benzoic acid; In toluene; at 100 ℃; for 14h; Overall yield = 89 %; Overall yield = 217 mg;
DOI:10.1002/chem.201503744