PtMe₂(1,2-bis(4-methoxyphenyl)-3,4-bis[(2,4,6-tri-tert-butylphenyl)phosphinidene]cyclobutene)

Base Information

• Chemical Name: PtMe₂(1,2-bis(4-methoxyphenyl)-3,4-bis[(2,4,6-tri-tert-butylphenyl)phosphinidene]cyclobutene)
• CAS No.: 384366-89-6
• Molecular Formula: C₅₆H₇₈O₂P₂Pt
• Molecular Weight: 1040.26

Synonyms:PtMe₂(1,2-bis(4-methoxyphenyl)-3,4-bis[(2,4,6-tri-tert-butylphenyl)phosphinidene]cyclobutene)

Chemical Property of PtMe₂(1,2-bis(4-methoxyphenyl)-3,4-bis[(2,4,6-tri-tert-butylphenyl)phosphinidene]cyclobutene)

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Technology Process of PtMe₂(1,2-bis(4-methoxyphenyl)-3,4-bis[(2,4,6-tri-tert-butylphenyl)phosphinidene]cyclobutene)

There total 1 articles about PtMe₂(1,2-bis(4-methoxyphenyl)-3,4-bis[(2,4,6-tri-tert-butylphenyl)phosphinidene]cyclobutene) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

bis[dimethyl(μ-dimethylsulfide)platinum(II)] + 1,2-bis(4-methoxyphenyl)-3,4-bis[(2,4,6-tri-tert-butylphenyl)phosphinidene]cyclobutene (359715-86-9) → PtMe2(1,2-bis(4-methoxyphenyl)-3,4-bis[(2,4,6-tri-tert-butylphenyl)phosphinidene]cyclobutene) (384366-89-6)

Guidance literature:

In diethyl ether; (N2); addn. of ligand to a suspn. of platinum complex in Et2O, stirring at room temp. for 12 h in the dark; evapn., washing with Et2O, drying in vac.; elem. anal.;

DOI:10.1021/om030676d

Reference yield: 89.0%

PtMe2(1,2-bis(4-methoxyphenyl)-3,4-bis[(2,4,6-tri-tert-butylphenyl)phosphinidene]cyclobutene) (384366-89-6) + trifluorormethanesulfonic acid (1493-13-6) → PtMe(OTf)(1,2-bis(4-methoxyphenyl)-3,4-bis[(2,4,6-tri-tert-butylphenyl)phosphinidene]cyclobutene) (384366-64-7)

Guidance literature:

In diethyl ether; (N2); addn. of a soln. of acid in Et2O to a suspn. of platinum complex in Et2O at 0°C, warming to room temp., stirring for 3 h in the dark; filtration, washing with Et2O, drying in vac.; elem. anal.;

DOI:10.1021/om030676d

upstream raw materials:

1,2-bis(4-methoxyphenyl)-3,4-bis[(2,4,6-tri-tert-butylphenyl)phosphinidene]cyclobutene

Downstream raw materials:

PtMe(OTf)(1,2-bis(4-methoxyphenyl)-3,4-bis[(2,4,6-tri-tert-butylphenyl)phosphinidene]cyclobutene)

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