diisopropyl(2-(2-phenylnaphthalen-1-yl)phenyl)phosphine oxide

Base Information

Chemical Name:diisopropyl(2-(2-phenylnaphthalen-1-yl)phenyl)phosphine oxide
CAS No.:1558012-02-4
Molecular Formula:C₂₈H₂₉OP
Molecular Weight:412.511
Hs Code.:

Synonyms:diisopropyl(2-(2-phenylnaphthalen-1-yl)phenyl)phosphine oxide

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Chemical Property of diisopropyl(2-(2-phenylnaphthalen-1-yl)phenyl)phosphine oxide

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Technology Process of diisopropyl(2-(2-phenylnaphthalen-1-yl)phenyl)phosphine oxide

There total 6 articles about diisopropyl(2-(2-phenylnaphthalen-1-yl)phenyl)phosphine oxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

: 1558012-16-0
C₂₂H₂₅OP

: 66003-76-7
Diphenyliodonium triflate

: 1558012-02-4
diisopropyl(2-(2-phenylnaphthalen-1-yl)phenyl)phosphine oxide

Guidance literature:: With silver carbonate; palladium dichloride; Trimethylacetic acid; In N,N-dimethyl-formamide; at 80 ℃; for 36h; regioselective reaction;
DOI:10.1039/c3cc49050e

Reference yield:

: 18937-92-3
1-(2-bromophenyl)naphthalene

: 1558012-02-4
diisopropyl(2-(2-phenylnaphthalen-1-yl)phenyl)phosphine oxide

Guidance literature:: Multi-step reaction with 3 steps

1.1: n-butyllithium / hexane; diethyl ether / 2 h / 0 °C

1.2: 1 h / 20 °C

2.1: dihydrogen peroxide / water; methanol / 1 h / 20 °C

3.1: palladium dichloride; silver carbonate; Trimethylacetic acid / N,N-dimethyl-formamide / 36 h / 80 °C

With n-butyllithium; dihydrogen peroxide; silver carbonate; palladium dichloride; Trimethylacetic acid; In methanol; diethyl ether; hexane; water; N,N-dimethyl-formamide;
DOI:10.1039/c3cc49050e

Reference yield:

: 583-55-1
1-Bromo-2-iodobenzene

: 1558012-02-4
diisopropyl(2-(2-phenylnaphthalen-1-yl)phenyl)phosphine oxide

Guidance literature:: Multi-step reaction with 4 steps

1.1: bis-triphenylphosphine-palladium(II) chloride; potassium carbonate / 1,2-dimethoxyethane; water / 5 h / 80 °C / Inert atmosphere

2.1: n-butyllithium / hexane; diethyl ether / 2 h / 0 °C

2.2: 1 h / 20 °C

3.1: dihydrogen peroxide / water; methanol / 1 h / 20 °C

4.1: palladium dichloride; silver carbonate; Trimethylacetic acid / N,N-dimethyl-formamide / 36 h / 80 °C

With bis-triphenylphosphine-palladium(II) chloride; n-butyllithium; dihydrogen peroxide; potassium carbonate; silver carbonate; palladium dichloride; Trimethylacetic acid; In methanol; 1,2-dimethoxyethane; diethyl ether; hexane; water; N,N-dimethyl-formamide;
DOI:10.1039/c3cc49050e