5-(3,4-dichlorobenzylidene)-1,3-dimethyl-2,4,6(1H,3H,5H)pyrimidinetrione

Base Information

• Chemical Name: 5-(3,4-dichlorobenzylidene)-1,3-dimethyl-2,4,6(1H,3H,5H)pyrimidinetrione
• CAS No.: 57280-35-0
• Molecular Formula: C₁₃H₁₀Cl₂N₂O₃
• Molecular Weight: 313.14

Synonyms:5-(3,4-dichlorobenzylidene)-1,3-dimethyl-2,4,6(1H,3H,5H)pyrimidinetrione

Chemical Property of 5-(3,4-dichlorobenzylidene)-1,3-dimethyl-2,4,6(1H,3H,5H)pyrimidinetrione

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 5-(3,4-dichlorobenzylidene)-1,3-dimethyl-2,4,6(1H,3H,5H)pyrimidinetrione

There total 2 articles about 5-(3,4-dichlorobenzylidene)-1,3-dimethyl-2,4,6(1H,3H,5H)pyrimidinetrione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

1,3-dimethylbarbituric acid (769-42-6) + 3,4-dichlorobenzaldehyde (6287-38-3) → 5-(3,4-dichlorobenzylidene)-1,3-dimethyl-2,4,6(1H,3H,5H)pyrimidinetrione (57280-35-0)

Guidance literature:

In water; at 100 ℃; for 0.5h;

DOI:10.2174/157340611795564231

Reference yield:

→ 5-(3,4-dichlorobenzylidene)-1,3-dimethyl-2,4,6(1H,3H,5H)pyrimidinetrione (57280-35-0)

Guidance literature:

entspr. 6-(Benzylidenhydrazino)uracil (1t), H2SO4;

DOI:10.1246/bcsj.48.1484

Reference yield: 88.0%

indole-2,3-dione (91-56-5,1186480-61-4,84788-92-1) + 5-(3,4-dichlorobenzylidene)-1,3-dimethyl-2,4,6(1H,3H,5H)pyrimidinetrione (57280-35-0) + L-thioproline (34592-47-7,2756-91-4,6070-92-4,60731-25-1) → 1,3-dimethyl-5'-(3,4-dichlorophenyl)-7'-(spiro-3''-indolino)tetrahydro-1H,1'H-spiro[pyrimidine-5,6'-pyrrolo[1,2-c]thiazole]-2,4,6-trione

Guidance literature:

In ethanol; for 1.5h; regioselective reaction; Reflux;

DOI:10.3390/molecules171112704

upstream raw materials:

1,3-dimethylbarbituric acid

3,4-dichlorobenzaldehyde

Post a RFQ

Cas No.:

Product Name:

Quantity:

Please select Metric Ton KG G Pound L ML

Email:

Company name:

Valid Period:

Detailed Requirements:

• Sample
• MOQ
• GMP
• FDA
• Price
  FOB CIF CFR EXW
• Urgent purchase

Enter 15 to 2000 letters.Word count: 0 letters

Attach files(File Format: Jpeg, Jpg, Gif, Png, PDF, PPT, Zip, Rar,Word or Excel Maximum File Size: 3MB)

Remove

Submit

1

What can I do for you?
Get Best Price

Get Best Price for 57280-35-0 5-(3,4-dichlorobenzylidene)-1,3-dimethyl-2,4,6(1H,3H,5H)pyrimidinetrione

Send

Send

Metric Ton KG G Pound L ML

Send

Send