C₂₂H₂₂O₅

Base Information

Chemical Name:C₂₂H₂₂O₅
CAS No.:1342299-88-0
Molecular Formula:C₂₂H₂₂O₅
Molecular Weight:366.414
Hs Code.:

C<sub>22</sub>H<sub>22</sub>O<sub>5</sub>

Synonyms:C₂₂H₂₂O₅

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Chemical Property of C₂₂H₂₂O₅

Chemical Property:

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Technology Process of C₂₂H₂₂O₅

There total 11 articles about C₂₂H₂₂O₅ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 34133-58-9
4-hydroxy-isophthalonitrile

: 1342299-88-0
C₂₂H₂₂O₅

Guidance literature:: Multi-step reaction with 10 steps

1.1: water; sulfuric acid / 13 h / 135 °C

1.2: 1.5 h / 95 °C

2.1: N-Bromosuccinimide / tetrahydrofuran / 2.5 h / 0 - 20 °C

3.1: pyridine / 14 h / 140 °C

4.1: potassium carbonate / N,N-dimethyl-formamide / 13.5 h / 110 °C / Inert atmosphere

5.1: dmap; triethylamine / dichloromethane; tetrahydrofuran / 3.25 h / 50 °C

6.1: triethylamine / triphenylphosphine; palladium diacetate / 2 h / 95 °C

6.2: 1 h / 20 °C

7.1: potassium carbonate / 4 h / 20 °C

8.1: pyridine / 14.5 h / 140 °C

9.1: potassium hydrogencarbonate / N,N-dimethyl-formamide / 20.33 h

10.1: potassium carbonate / N,N-dimethyl-formamide / 13 h / 60 °C

With pyridine; dmap; N-Bromosuccinimide; sulfuric acid; water; potassium carbonate; potassium hydrogencarbonate; triethylamine; palladium diacetate; triphenylphosphine; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;

Reference yield:

: 1342299-87-9
C₁₉H₁₈O₅

: 106-95-6
allyl bromide

: 1342299-88-0
C₂₂H₂₂O₅

Guidance literature:: With potassium carbonate; In N,N-dimethyl-formamide; at 60 ℃; for 13h;

Reference yield:

: 5985-24-0
dimethyl 4-hydroxyisophthalate

: 1342299-88-0
C₂₂H₂₂O₅

Guidance literature:: Multi-step reaction with 9 steps

1.1: N-Bromosuccinimide / tetrahydrofuran / 2.5 h / 0 - 20 °C

2.1: pyridine / 14 h / 140 °C

3.1: potassium carbonate / N,N-dimethyl-formamide / 13.5 h / 110 °C / Inert atmosphere

4.1: dmap; triethylamine / dichloromethane; tetrahydrofuran / 3.25 h / 50 °C

5.1: triethylamine / triphenylphosphine; palladium diacetate / 2 h / 95 °C

5.2: 1 h / 20 °C

6.1: potassium carbonate / 4 h / 20 °C

7.1: pyridine / 14.5 h / 140 °C

8.1: potassium hydrogencarbonate / N,N-dimethyl-formamide / 20.33 h

9.1: potassium carbonate / N,N-dimethyl-formamide / 13 h / 60 °C

With pyridine; dmap; N-Bromosuccinimide; potassium carbonate; potassium hydrogencarbonate; triethylamine; palladium diacetate; triphenylphosphine; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;