(2E)-3-(4-chlorophenyl)-1-(2,3-dihydro-1,4-benzodioxin-6-yl)prop-2-en-1-one

Base Information

Chemical Name:(2E)-3-(4-chlorophenyl)-1-(2,3-dihydro-1,4-benzodioxin-6-yl)prop-2-en-1-one
CAS No.:343610-44-6
Molecular Formula:C₁₇H₁₃ClO₃
Molecular Weight:300.741
Hs Code.:

Synonyms:(2E)-3-(4-chlorophenyl)-1-(2,3-dihydro-1,4-benzodioxin-6-yl)prop-2-en-1-one

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (2E)-3-(4-chlorophenyl)-1-(2,3-dihydro-1,4-benzodioxin-6-yl)prop-2-en-1-one

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Technology Process of (2E)-3-(4-chlorophenyl)-1-(2,3-dihydro-1,4-benzodioxin-6-yl)prop-2-en-1-one

There total 3 articles about (2E)-3-(4-chlorophenyl)-1-(2,3-dihydro-1,4-benzodioxin-6-yl)prop-2-en-1-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 2879-20-1
1,4-benzodioxan-6-yl methyl ketone

: 104-88-1
4-chlorobenzaldehyde

: 343610-44-6
(2E)-3-(4-chlorophenyl)-1-(2,3-dihydro-1,4-benzodioxin-6-yl)prop-2-en-1-one

Guidance literature:: With potassium hydroxide; In ethanol; for 10h;
DOI:10.1016/j.bioorg.2019.103335

Reference yield: 80.0%

: 4629-54-3
2-bromo-1-(2,3-dihydro-1,4-benzodioxin-6-yl)ethanone

: 104-88-1
4-chlorobenzaldehyde

: 343610-44-6
(2E)-3-(4-chlorophenyl)-1-(2,3-dihydro-1,4-benzodioxin-6-yl)prop-2-en-1-one

Guidance literature:: With phenylsilane; N-ethyl-N,N-diisopropylamine; 1-(n-butyl)phospholane-1-oxide; 4-nitro-benzoic acid; In ethyl acetate; at 20 ℃; for 24h; diastereoselective reaction; Inert atmosphere; Sealed tube; Schlenk technique;
DOI:10.1002/chem.201300546

Reference yield: 80.0%

: 343610-44-6
(2E)-3-(4-chlorophenyl)-1-(2,3-dihydro-1,4-benzodioxin-6-yl)prop-2-en-1-one

Guidance literature:: With N-ethyl-N,N-diisopropylamine; 1-(n-butyl)phospholane-1-oxide; 4-nitro-benzoic acid; In ethyl acetate; for 0.0166667h; Inert atmosphere; Schlenk technique; Sealed tube;

With phenylsilane; In ethyl acetate; at 20 ℃; for 24h; Inert atmosphere;