sulfamic acid 5-[4-(tert-butyl-dimethyl-silanyloxy)-phenyl]-pentyl ester

Base Information

• Chemical Name: sulfamic acid 5-[4-(tert-butyl-dimethyl-silanyloxy)-phenyl]-pentyl ester
• CAS No.: 261634-36-0
• Molecular Formula: C₁₇H₃₁NO₄SSi
• Molecular Weight: 373.589
• Mol file: 261634-36-0.mol

Synonyms:sulfamic acid 5-[4-(tert-butyl-dimethyl-silanyloxy)-phenyl]-pentyl ester

Chemical Property of sulfamic acid 5-[4-(tert-butyl-dimethyl-silanyloxy)-phenyl]-pentyl ester

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of sulfamic acid 5-[4-(tert-butyl-dimethyl-silanyloxy)-phenyl]-pentyl ester

There total 2 articles about sulfamic acid 5-[4-(tert-butyl-dimethyl-silanyloxy)-phenyl]-pentyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

(polystyrene resin Novabiochem)-C6H4(C6H5)2CNHSO2O(CH2)5C6H4OSi(CH3)2(C4H9) → sulfamic acid 5-[4-(tert-butyl-dimethyl-silanyloxy)-phenyl]-pentyl ester (261634-36-0)

Guidance literature:

With trifluoroacetic acid; In dichloromethane; for 3h;

DOI:10.1021/ol990381p

Reference yield:

trityl-sulfamic acid 5-[4-(tert-butyl-dimethyl-silanyloxy)-phenyl]-pentyl ester → sulfamic acid 5-[4-(tert-butyl-dimethyl-silanyloxy)-phenyl]-pentyl ester (261634-36-0)

Guidance literature:

With trifluoroacetic acid; In dichloromethane; for 1h;

DOI:10.1021/ol990381p

Reference yield: 96.0%

trityl chloride (76-83-5) + sulfamic acid 5-[4-(tert-butyl-dimethyl-silanyloxy)-phenyl]-pentyl ester (261634-36-0) → trityl-sulfamic acid 5-[4-(tert-butyl-dimethyl-silanyloxy)-phenyl]-pentyl ester

Guidance literature:

With N-ethyl-N,N-diisopropylamine; In dichloromethane;

DOI:10.1021/ol990381p