(C₅(CH₃)5)Ru(H)(CCCH₂(OH))(P(CH₂CH₃)3)2⁽¹⁺⁾*B(C₆H₅)4^(1-)=[Ru(H)(C₁₀H₁₅)(C₃H₃O)(P(C₂H₅)3)2][B(C₆H₅)4]

Base Information

• Chemical Name: (C₅(CH₃)5)Ru(H)(CCCH₂(OH))(P(CH₂CH₃)3)2⁽¹⁺⁾*B(C₆H₅)4^(1-)=[Ru(H)(C₁₀H₁₅)(C₃H₃O)(P(C₂H₅)3)2][B(C₆H₅)4]
• CAS No.: 251480-54-3
• Molecular Formula: C₂₄H₂₀B*C₂₅H₄₉OP₂Ru
• Molecular Weight: 847.915

Synonyms:(C₅(CH₃)5)Ru(H)(CCCH₂(OH))(P(CH₂CH₃)3)2⁽¹⁺⁾*B(C₆H₅)4^(1-)=[Ru(H)(C₁₀H₁₅)(C₃H₃O)(P(C₂H₅)3)2][B(C₆H₅)4]

Chemical Property of (C₅(CH₃)5)Ru(H)(CCCH₂(OH))(P(CH₂CH₃)3)2⁽¹⁺⁾*B(C₆H₅)4^(1-)=[Ru(H)(C₁₀H₁₅)(C₃H₃O)(P(C₂H₅)3)2][B(C₆H₅)4]

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Technology Process of (C₅(CH₃)5)Ru(H)(CCCH₂(OH))(P(CH₂CH₃)3)2⁽¹⁺⁾*B(C₆H₅)4^(1-)=[Ru(H)(C₁₀H₁₅)(C₃H₃O)(P(C₂H₅)3)2][B(C₆H₅)4]

There total 1 articles about (C₅(CH₃)5)Ru(H)(CCCH₂(OH))(P(CH₂CH₃)3)2⁽¹⁺⁾*B(C₆H₅)4^(1-)=[Ru(H)(C₁₀H₁₅)(C₃H₃O)(P(C₂H₅)3)2][B(C₆H₅)4] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

Cp(*)(triethylphosphine)2RuCl + sodium tetraphenyl borate (143-66-8) + propargyl alcohol (107-19-7) → (C5(CH3)5)Ru(H)(CCCH2(OH))(P(CH2CH3)3)2(1+)*B(C6H5)4(1-)=[Ru(H)(C10H15)(C3H3O)(P(C2H5)3)2][B(C6H5)4] (251480-54-3)

Guidance literature:

In methanol; addn. of Ru-complex to soln. of alcohol (excess) and NaBPh4 (excess) at 0°C; warming; pptn.; filtration; washing (cold EtOH, hexane);

DOI:10.1021/om980970j

Reference yield: 100.0%

(C5(CH3)5)Ru(H)(CCCH2(OH))(P(CH2CH3)3)2(1+)*B(C6H5)4(1-)=[Ru(H)(C10H15)(C3H3O)(P(C2H5)3)2][B(C6H5)4] (251480-54-3) → [Cp(*)(triethylphosphine)2Ru(=C=CH-CH2OH)][tetraphenylborate] (251480-68-9)

Guidance literature:

In solid; heating (30-35°C, 3 h);

DOI:10.1021/om980970j

upstream raw materials:

sodium tetraphenyl borate

propargyl alcohol

Downstream raw materials:

[Cp(*)(triethylphosphine)2Ru(=C=CH-CH₂OH)][tetraphenylborate]

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