(3S)-3--2-n-butyl-hept-1-ene

Base Information

Chemical Name:(3S)-3--2-n-butyl-hept-1-ene
CAS No.:150062-23-0
Molecular Formula:C₂₆H₃₇NO₃S
Molecular Weight:443.651
Hs Code.:

(3S)-3-<N-(4-Methoxybenzyl)-N-tosylamino>-2-n-butyl-hept-1-ene

Synonyms:(3S)-3--2-n-butyl-hept-1-ene

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (3S)-3--2-n-butyl-hept-1-ene

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Technology Process of (3S)-3--2-n-butyl-hept-1-ene

There total 1 articles about (3S)-3--2-n-butyl-hept-1-ene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 824-94-2
p-methoxybenzyl chloride

: 150062-20-7
(3S)-3-(N-Tosylamino)-2-n-butylhept-1-ene

: 150062-23-0
(3S)-3--2-n-butyl-hept-1-ene

Guidance literature:: With potassium carbonate; tetra-(n-butyl)ammonium iodide; In acetone; for 10h; Heating;
DOI:10.1021/jo00069a052

Reference yield:

: 150062-23-0
(3S)-3--2-n-butyl-hept-1-ene

: 150062-30-9
(3S)-syn-2-n-Butyl-3-(N-tosylamino)heptan-1-ol

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) BH₃*THF, 2.) 3M NaOH, 30percent H₂O₂ / 1.) THF, -78 deg C, 2 h; -26 deg C, 24 h, 2.) EtOH, 25 deg C, 10 h

2: 92 percent / (NH₄)2Ce(NO₃)6 / acetonitrile; H₂O / 0.17 h / 25 °C

With sodium hydroxide; borane-THF; ammonium cerium(IV) nitrate; dihydrogen peroxide; In water; acetonitrile;
DOI:10.1021/jo00069a052

Reference yield:

: 150062-23-0
(3S)-3--2-n-butyl-hept-1-ene

: 150062-29-6
(3S)-anti-2-n-Butyl-3-(N-tosylamino)heptan-1-ol

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) BH₃*THF, 2.) 3M NaOH, 30percent H₂O₂ / 1.) THF, -78 deg C, 2 h; -26 deg C, 24 h, 2.) EtOH, 25 deg C, 10 h

2: 70 percent / (NH₄)2Ce(NO₃)6 / acetonitrile; H₂O / 0.17 h / 25 °C

With sodium hydroxide; borane-THF; ammonium cerium(IV) nitrate; dihydrogen peroxide; In water; acetonitrile;
DOI:10.1021/jo00069a052