N-(1-Methyl-3-phenyl-2-propenylidene)aniline

Base Information

Chemical Name:N-(1-Methyl-3-phenyl-2-propenylidene)aniline
CAS No.:17424-79-2
Molecular Formula:C16H15 N
Molecular Weight:221.302
Hs Code.:
NSC Number:320238,155601
Nikkaji Number:J1.322.848E,J1.399.249E,J2.803.042H

Synonyms:N-(1-Methyl-3-phenyl-2-propenylidene)aniline;NSC155601;NSC 155601;17424-79-2;(E)-N,4-diphenylbut-3-en-2-imine;Benzenamine, (E,?)-;N,4-Diphenyl-3-butene-2-imine;NSC320238;NSC-155601;NSC-320238;(3E)-N,4-Diphenyl-3-butene-2-imine;(E)-N-((E)-4-phenylbut-3-en-2-ylidene)aniline;N-[(1E,2E)-1-Methyl-3-phenylallylidene]aniline;Benzenamine, N-(1-methyl-3-phenyl-2-propenylidene)-;N-(1-Methyl-3-phenyl-2-propenylidene)-N-phenylamine

Suppliers and Price of N-(1-Methyl-3-phenyl-2-propenylidene)aniline

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 4 raw suppliers

Chemical Property of N-(1-Methyl-3-phenyl-2-propenylidene)aniline

Chemical Property:

Vapor Pressure:0.000203mmHg at 25°C
Boiling Point:337.6°C at 760 mmHg
Flash Point:150.1°C
Density:0.93g/cm³
XLogP3:3.9
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:3
Exact Mass:221.120449483
Heavy Atom Count:17
Complexity:265

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC(=NC1=CC=CC=C1)C=CC2=CC=CC=C2
Isomeric SMILES:CC(=NC1=CC=CC=C1)/C=C/C2=CC=CC=C2

Technology Process of N-(1-Methyl-3-phenyl-2-propenylidene)aniline

There total 2 articles about N-(1-Methyl-3-phenyl-2-propenylidene)aniline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 62-53-3
aniline

: 122-57-6
1-Phenylbut-1-en-3-one

: 17424-79-2
2-methyl-1,4-diphenyl-1-aza-1,3-butadiene

Guidance literature:: With zinc(II) chloride; In benzene; for 6h; Reflux;
DOI:10.1016/j.tet.2011.01.067

Reference yield:

: 17424-79-2
2-methyl-1,4-diphenyl-1-aza-1,3-butadiene

Guidance literature:: 2-Anilino-2-methyl-4-phenyl-but-3-ennitril (Ig) m. methanol. KOH;

Reference yield: 97.0%

: 109-72-8,29786-93-4
n-butyllithium

: 17424-79-2
2-methyl-1,4-diphenyl-1-aza-1,3-butadiene

: 1291104-80-7
N-(3-methyl-1-phenylhept-1-en-3-yl)aniline

Guidance literature:: n-butyllithium; 2-methyl-1,4-diphenyl-1-aza-1,3-butadiene; With lithium bromide; In 2-methyltetrahydrofuran; hexane; at 0 ℃; for 2h;

With ammonium chloride; In 2-methyltetrahydrofuran; hexane; water; at 0 ℃; regioselective reaction;
DOI:10.1016/j.tet.2011.01.067