1-(4-chlorophenyl)-N'-(3-(2-hydroxypropan-2-yl)pyridin-2-yl)cyclopropanecarbohydrazide

Base Information

Chemical Name:1-(4-chlorophenyl)-N'-(3-(2-hydroxypropan-2-yl)pyridin-2-yl)cyclopropanecarbohydrazide
CAS No.:1140898-88-9
Molecular Formula:C₁₈H₂₀ClN₃O₂
Molecular Weight:345.829
Hs Code.:

Synonyms:1-(4-chlorophenyl)-N'-(3-(2-hydroxypropan-2-yl)pyridin-2-yl)cyclopropanecarbohydrazide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-(4-chlorophenyl)-N'-(3-(2-hydroxypropan-2-yl)pyridin-2-yl)cyclopropanecarbohydrazide

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Technology Process of 1-(4-chlorophenyl)-N'-(3-(2-hydroxypropan-2-yl)pyridin-2-yl)cyclopropanecarbohydrazide

There total 1 articles about 1-(4-chlorophenyl)-N'-(3-(2-hydroxypropan-2-yl)pyridin-2-yl)cyclopropanecarbohydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

2-(2-hydrazinylpyridin-3-yl)propan-2-ol hydrochloride: 1140898-86-7
2-(2-hydrazinylpyridin-3-yl)propan-2-ol hydrochloride

: 72934-37-3
3-(4-chlorophenyl)-1-cyclopropanecarboxylic acid

1-(4-chlorophenyl)-N'-(3-(2-hydroxypropan-2-yl)pyridin-2-yl)cyclopropanecarbohydrazide: 1140898-88-9
1-(4-chlorophenyl)-N'-(3-(2-hydroxypropan-2-yl)pyridin-2-yl)cyclopropanecarbohydrazide

Guidance literature:: 3-(4-chlorophenyl)-1-cyclopropanecarboxylic acid; With oxalyl dichloride; N,N-dimethyl-formamide; In toluene; at 20 - 25 ℃; for 4.41667h;

2-(2-hydrazinylpyridin-3-yl)propan-2-ol hydrochloride; With potassium carbonate; In tetrahydrofuran; water; toluene; at 5 ℃; for 1.08333h;

Reference yield:

1-(4-chlorophenyl)-N'-(3-(2-hydroxypropan-2-yl)pyridin-2-yl)cyclopropanecarbohydrazide: 1140898-88-9
1-(4-chlorophenyl)-N'-(3-(2-hydroxypropan-2-yl)pyridin-2-yl)cyclopropanecarbohydrazide

: 1140898-92-5
3-(1-(4-chlorophenyl)cyclopropyl)-8-(prop-1-en-2-yl)-[1,2,4]triazolo[4,3-a]pyridine hydrochloride

Guidance literature:: 1-(4-chlorophenyl)-N'-(3-(2-hydroxypropan-2-yl)pyridin-2-yl)cyclopropanecarbohydrazide; With trichlorophosphate; In toluene; at 95 ℃; for 22.0833h;

With potassium carbonate; In water; toluene; acetonitrile; at 5 - 20 ℃; for 18h;

With hydrogenchloride; In water; isopropyl alcohol; toluene; at 20 ℃; for 18.25h;

Reference yield:

1-(4-chlorophenyl)-N'-(3-(2-hydroxypropan-2-yl)pyridin-2-yl)cyclopropanecarbohydrazide: 1140898-88-9
1-(4-chlorophenyl)-N'-(3-(2-hydroxypropan-2-yl)pyridin-2-yl)cyclopropanecarbohydrazide

: 1140898-87-8
2-(3-(1-(4-chlorophenyl)cyclopropyl)-[1,2,4]triazolo[4,3-a]pyridin-8-yl)propan-2-ol hydrochloride

Guidance literature:: 1-(4-chlorophenyl)-N'-(3-(2-hydroxypropan-2-yl)pyridin-2-yl)cyclopropanecarbohydrazide; With acetic acid; In toluene; at 100 - 105 ℃; for 24 - 35h;

With hydrogenchloride; In water; isopropyl alcohol; toluene; at 20 ℃; for 16.05 - 16.1667h; Product distribution / selectivity;