Technology Process of C44H48ClNO6
There total 3 articles about C44H48ClNO6 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
diethylamine;
In
acetonitrile;
at 20 ℃;
for 5h;
Inert atmosphere;
DOI:10.1002/chem.201003721
- Guidance literature:
-
Multi-step reaction with 3 steps
1: diethylamino-sulfur trifluoride / dichloromethane / -78 - -60 °C / Inert atmosphere
2: trimethylsilyl trifluoromethanesulfonate / dichloromethane / 2.5 h / -30 - 20 °C / Molecular sieve; Inert atmosphere
3: diethylamine / acetonitrile / 5 h / 20 °C / Inert atmosphere
With
diethylamino-sulfur trifluoride; trimethylsilyl trifluoromethanesulfonate; diethylamine;
In
dichloromethane; acetonitrile;
DOI:10.1002/chem.201003721
- Guidance literature:
-
Multi-step reaction with 2 steps
1: trimethylsilyl trifluoromethanesulfonate / dichloromethane / 2.5 h / -30 - 20 °C / Molecular sieve; Inert atmosphere
2: diethylamine / acetonitrile / 5 h / 20 °C / Inert atmosphere
With
trimethylsilyl trifluoromethanesulfonate; diethylamine;
In
dichloromethane; acetonitrile;
DOI:10.1002/chem.201003721