Technology Process of C32H26N8O6
There total 4 articles about C32H26N8O6 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
copper(l) iodide; N-ethyl-N,N-diisopropylamine;
In
acetonitrile;
at 20 ℃;
for 16h;
Inert atmosphere;
DOI:10.1039/c2ob27155a
- Guidance literature:
-
Multi-step reaction with 4 steps
1: oxalyl dichloride / dichloromethane / 5 h / 20 °C / Inert atmosphere
2: triethylamine / N,N-dimethyl-formamide / 2 h / 20 °C / Inert atmosphere
3: sodium azide; copper(l) iodide; sodium L-ascorbate; N,N`-dimethylethylenediamine / dimethyl sulfoxide; water / 16 h / 20 °C / Inert atmosphere
4: copper(l) iodide; N-ethyl-N,N-diisopropylamine / acetonitrile / 16 h / 20 °C / Inert atmosphere
With
copper(l) iodide; sodium azide; oxalyl dichloride; sodium L-ascorbate; triethylamine; N-ethyl-N,N-diisopropylamine; N,N`-dimethylethylenediamine;
In
dichloromethane; water; dimethyl sulfoxide; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1039/c2ob27155a
- Guidance literature:
-
Multi-step reaction with 2 steps
1: sodium azide; copper(l) iodide; sodium L-ascorbate; N,N`-dimethylethylenediamine / dimethyl sulfoxide; water / 16 h / 20 °C / Inert atmosphere
2: copper(l) iodide; N-ethyl-N,N-diisopropylamine / acetonitrile / 16 h / 20 °C / Inert atmosphere
With
copper(l) iodide; sodium azide; sodium L-ascorbate; N-ethyl-N,N-diisopropylamine; N,N`-dimethylethylenediamine;
In
water; dimethyl sulfoxide; acetonitrile;
DOI:10.1039/c2ob27155a
