rac-1-[4-(di-tert-butylfluorosilyl)benzyl]-4-(tetrahydro-2H-pyran-2-yl-oxymethyl)-1H-1,2,3-triazole

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Chemical Name:rac-1-[4-(di-tert-butylfluorosilyl)benzyl]-4-(tetrahydro-2H-pyran-2-yl-oxymethyl)-1H-1,2,3-triazole
CAS No.:1333414-92-8
Molecular Formula:C₂₃H₃₆FN₃O₂Si
Molecular Weight:433.642
Hs Code.:

Synonyms:rac-1-[4-(di-tert-butylfluorosilyl)benzyl]-4-(tetrahydro-2H-pyran-2-yl-oxymethyl)-1H-1,2,3-triazole

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Chemical Property of rac-1-[4-(di-tert-butylfluorosilyl)benzyl]-4-(tetrahydro-2H-pyran-2-yl-oxymethyl)-1H-1,2,3-triazole

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Technology Process of rac-1-[4-(di-tert-butylfluorosilyl)benzyl]-4-(tetrahydro-2H-pyran-2-yl-oxymethyl)-1H-1,2,3-triazole

There total 2 articles about rac-1-[4-(di-tert-butylfluorosilyl)benzyl]-4-(tetrahydro-2H-pyran-2-yl-oxymethyl)-1H-1,2,3-triazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 6089-04-9
3-(tetrahydropyran-2'-yloxy)propyne

: 1333414-88-2
4-(di-tert-butylfluorosilyl)benzylazide

: 1333414-92-8
rac-1-[4-(di-tert-butylfluorosilyl)benzyl]-4-(tetrahydro-2H-pyran-2-yl-oxymethyl)-1H-1,2,3-triazole

Guidance literature:: With copper(ll) sulfate pentahydrate; sodium L-ascorbate; In water; tert-butyl alcohol; at 20 ℃; for 0.5h; chemoselective reaction; Inert atmosphere;
DOI:10.1055/s-0030-1260942

Reference yield:

: 1146956-36-6
4-(di-tert-butylfluorosilanyl)benzyl alcohol

: 1333414-92-8
rac-1-[4-(di-tert-butylfluorosilyl)benzyl]-4-(tetrahydro-2H-pyran-2-yl-oxymethyl)-1H-1,2,3-triazole

Guidance literature:: Multi-step reaction with 2 steps

1: diphenyl phosphoryl azide; 1,8-diazabicyclo[5.4.0]undec-7-ene / toluene / 13 h / 50 °C / Inert atmosphere

2: copper(ll) sulfate pentahydrate; sodium L-ascorbate / water; tert-butyl alcohol / 0.5 h / 20 °C / Inert atmosphere

With copper(ll) sulfate pentahydrate; diphenyl phosphoryl azide; 1,8-diazabicyclo[5.4.0]undec-7-ene; sodium L-ascorbate; In water; toluene; tert-butyl alcohol;
DOI:10.1055/s-0030-1260942