cis-(S)-4-[4-(3-chlorophenyl)-2-oxo-2-λ5[1,3,2]dioxaphosphinan-2-ylaminomethyl-2,6-dimethylbenzyl]-2-isopropyl-1-phenol

Base Information

Chemical Name:cis-(S)-4-[4-(3-chlorophenyl)-2-oxo-2-λ5[1,3,2]dioxaphosphinan-2-ylaminomethyl-2,6-dimethylbenzyl]-2-isopropyl-1-phenol
CAS No.:1282618-46-5
Molecular Formula:C₂₈H₃₃ClNO₄P
Molecular Weight:514.001
Hs Code.:

Synonyms:cis-(S)-4-[4-(3-chlorophenyl)-2-oxo-2-λ5[1,3,2]dioxaphosphinan-2-ylaminomethyl-2,6-dimethylbenzyl]-2-isopropyl-1-phenol

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Chemical Property of cis-(S)-4-[4-(3-chlorophenyl)-2-oxo-2-λ5[1,3,2]dioxaphosphinan-2-ylaminomethyl-2,6-dimethylbenzyl]-2-isopropyl-1-phenol

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Technology Process of cis-(S)-4-[4-(3-chlorophenyl)-2-oxo-2-λ5[1,3,2]dioxaphosphinan-2-ylaminomethyl-2,6-dimethylbenzyl]-2-isopropyl-1-phenol

There total 3 articles about cis-(S)-4-[4-(3-chlorophenyl)-2-oxo-2-λ5[1,3,2]dioxaphosphinan-2-ylaminomethyl-2,6-dimethylbenzyl]-2-isopropyl-1-phenol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: trans-4-(3-chlorophenyl)-2-(4-nitrophenoxy)-2-oxido-1,3,2-dioxaphosphorinane

: 4-(4-aminomethyl-2,6-dimethylbenzyl)-2-isopropylphenol hydrochloride

: 1282618-46-5
cis-(S)-4-[4-(3-chlorophenyl)-2-oxo-2-λ5[1,3,2]dioxaphosphinan-2-ylaminomethyl-2,6-dimethylbenzyl]-2-isopropyl-1-phenol

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; at 0 - 20 ℃; for 2.33333h;

Reference yield:

: C₄₀H₄₃NO₂

: 1282618-46-5
cis-(S)-4-[4-(3-chlorophenyl)-2-oxo-2-λ5[1,3,2]dioxaphosphinan-2-ylaminomethyl-2,6-dimethylbenzyl]-2-isopropyl-1-phenol

Guidance literature:: Multi-step reaction with 2 steps

1: hydrogenchloride; water / methanol / 72 h / 0 - 20 °C

2: N-ethyl-N,N-diisopropylamine / tetrahydrofuran / 2.33 h / 0 - 20 °C

With hydrogenchloride; water; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; methanol;

Reference yield:

: 877218-24-1
3,5-dimethyl-4-(3'-isopropyl-4'-(methoxymethoxy)benzyl)benzyl bromide

: 1282618-46-5
cis-(S)-4-[4-(3-chlorophenyl)-2-oxo-2-λ5[1,3,2]dioxaphosphinan-2-ylaminomethyl-2,6-dimethylbenzyl]-2-isopropyl-1-phenol

Guidance literature:: Multi-step reaction with 3 steps

1: acetonitrile / 12 h / 20 °C

2: hydrogenchloride; water / methanol / 72 h / 0 - 20 °C

3: N-ethyl-N,N-diisopropylamine / tetrahydrofuran / 2.33 h / 0 - 20 °C

With hydrogenchloride; water; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; methanol; acetonitrile;