2-fluoro-4,5-[1,2-dicarba-closo-dodecaborano⁽¹²⁾]-1,3,2-dithiastibolane

Base Information

• Chemical Name: 2-fluoro-4,5-[1,2-dicarba-closo-dodecaborano⁽¹²⁾]-1,3,2-dithiastibolane
• CAS No.: 1579224-18-2
• Molecular Formula: C₂H₁₀B₁₀FS₂Sb
• Molecular Weight: 347.092

Synonyms:2-fluoro-4,5-[1,2-dicarba-closo-dodecaborano⁽¹²⁾]-1,3,2-dithiastibolane

Chemical Property of 2-fluoro-4,5-[1,2-dicarba-closo-dodecaborano⁽¹²⁾]-1,3,2-dithiastibolane

Chemical Property:

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Technology Process of 2-fluoro-4,5-[1,2-dicarba-closo-dodecaborano⁽¹²⁾]-1,3,2-dithiastibolane

There total 1 articles about 2-fluoro-4,5-[1,2-dicarba-closo-dodecaborano⁽¹²⁾]-1,3,2-dithiastibolane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-chloro-4,5-[1,2-dicarba-closo-dodecaborano(12)]-1,3,2-dithiaphospholane (1579224-13-7) → difluorophosphine (14984-74-8) + 2-fluoro-4,5-[1,2-dicarba-closo-dodecaborano(12)]-1,3,2-dithiaphospholane (1579224-17-1) + 2-fluoro-4,5-[1,2-dicarba-closo-dodecaborano(12)]-1,3,2-dithiastibolane (1579224-18-2) + trifluorophosphane (7783-55-3)

Guidance literature:

With 1,2-bis{(4,5-[1,2-dicarba-closo-dodecaborano⁽¹²⁾]-1,3,2-dithiaphospholan-2-yl)thio}-1,2-dicarba-closo-dodecaborane⁽¹²⁾; 1-{4,5-[1,2-dicarba-closo-dodecaborano⁽¹²⁾]-1,3,2-dithiaphospholan-2-yl}thio-2-mercapto-1,2-dicarba-closo-dodecaborane⁽¹²⁾; antimony(III) fluoride; In ⁽²⁾H₈-toluene; at 0 - 50 ℃; for 5h; Time; Temperature; Inert atmosphere;

DOI:10.1039/c3dt52753k

upstream raw materials:

2-chloro-4,5-[1,2-dicarba-closo-dodecaborano⁽¹²⁾]-1,3,2-dithiaphospholane

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