hexadecyl 4-O-(6-O-acetyl-2,3,4-tri-O-benzyl-β-D-galactopyranosyl)-6-O-acetyl-3-O-allyl-2-azido-2-deoxy-β-D-glucopyranoside

Base Information

Chemical Name:hexadecyl 4-O-(6-O-acetyl-2,3,4-tri-O-benzyl-β-D-galactopyranosyl)-6-O-acetyl-3-O-allyl-2-azido-2-deoxy-β-D-glucopyranoside
CAS No.:127529-58-2
Molecular Formula:C₅₆H₇₉N₃O₁₂
Molecular Weight:986.256
Hs Code.:

Synonyms:hexadecyl 4-O-(6-O-acetyl-2,3,4-tri-O-benzyl-β-D-galactopyranosyl)-6-O-acetyl-3-O-allyl-2-azido-2-deoxy-β-D-glucopyranoside

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Chemical Property of hexadecyl 4-O-(6-O-acetyl-2,3,4-tri-O-benzyl-β-D-galactopyranosyl)-6-O-acetyl-3-O-allyl-2-azido-2-deoxy-β-D-glucopyranoside

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Technology Process of hexadecyl 4-O-(6-O-acetyl-2,3,4-tri-O-benzyl-β-D-galactopyranosyl)-6-O-acetyl-3-O-allyl-2-azido-2-deoxy-β-D-glucopyranoside

There total 6 articles about hexadecyl 4-O-(6-O-acetyl-2,3,4-tri-O-benzyl-β-D-galactopyranosyl)-6-O-acetyl-3-O-allyl-2-azido-2-deoxy-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 47.0%

: 36653-82-4,124-29-8
1-Hexadecanol

: 127529-80-0
6-O-acetyl-3-O-allyl-2-azido-2-deoxy-4-O-(6-O-acetyl-2,3,4-tri-O-benzyl-β-D-galactopyranosyl)-α-D-glucopyranosyl bromide

: 127529-58-2
hexadecyl 4-O-(6-O-acetyl-2,3,4-tri-O-benzyl-β-D-galactopyranosyl)-6-O-acetyl-3-O-allyl-2-azido-2-deoxy-β-D-glucopyranoside

Guidance literature:: 4 A molecular sieve; silver silicate aluminate; In dichloromethane; toluene; at -40 ℃; for 1.5h;

Reference yield:

: 61236-82-6
6-O-acetyl-2,3,4-tri-O-benzyl-α-D-galactopyranosyl bromide

: 127529-58-2
hexadecyl 4-O-(6-O-acetyl-2,3,4-tri-O-benzyl-β-D-galactopyranosyl)-6-O-acetyl-3-O-allyl-2-azido-2-deoxy-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 5 steps

1: 65 percent / silver silicate aluminate, molecular sieves 4 Angstroem / toluene; CH₂Cl₂ / 2 h / -55 °C

2: 99 percent / acetic acid / trifluoroacetic acid / 3 h / 0 - 20 °C

3: 75 percent / piperidine / tetrahydrofuran / 20 h

4: 90 percent / oxalyl bromide / CHCl₃; dimethylformamide / 2 h / 0 - 20 °C

5: 47 percent / silver silicate aluminate, molecular sieves 4 Angstroem / CH₂Cl₂; toluene / 1.5 h / -40 °C

With piperidine; Oxalyl bromide; acetic acid; 4 A molecular sieve; silver silicate aluminate; In tetrahydrofuran; dichloromethane; chloroform; N,N-dimethyl-formamide; toluene; trifluoroacetic acid;

Reference yield:

: 1,6-anhydro-3-O-allyl-2-azido-2-deoxy-β-D-glucopyranose

: 127529-58-2
hexadecyl 4-O-(6-O-acetyl-2,3,4-tri-O-benzyl-β-D-galactopyranosyl)-6-O-acetyl-3-O-allyl-2-azido-2-deoxy-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 5 steps

1: 65 percent / silver silicate aluminate, molecular sieves 4 Angstroem / toluene; CH₂Cl₂ / 2 h / -55 °C

2: 99 percent / acetic acid / trifluoroacetic acid / 3 h / 0 - 20 °C

3: 75 percent / piperidine / tetrahydrofuran / 20 h

4: 90 percent / oxalyl bromide / CHCl₃; dimethylformamide / 2 h / 0 - 20 °C

5: 47 percent / silver silicate aluminate, molecular sieves 4 Angstroem / CH₂Cl₂; toluene / 1.5 h / -40 °C

With piperidine; Oxalyl bromide; acetic acid; 4 A molecular sieve; silver silicate aluminate; In tetrahydrofuran; dichloromethane; chloroform; N,N-dimethyl-formamide; toluene; trifluoroacetic acid;