2-<3-phenylacetamido-4-(m-acetamido)phenylthiocarbonate-(3R,4R)-azetidin-2-on-1-yl>-trichloroethyl acetate

Base Information

Chemical Name:2-<3-phenylacetamido-4-(m-acetamido)phenylthiocarbonate-(3R,4R)-azetidin-2-on-1-yl>-trichloroethyl acetate
CAS No.:122691-94-5
Molecular Formula:C₂₄H₂₂Cl₃N₃O₇S
Molecular Weight:602.88
Hs Code.:

Synonyms:2-<3-phenylacetamido-4-(m-acetamido)phenylthiocarbonate-(3R,4R)-azetidin-2-on-1-yl>-trichloroethyl acetate

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Chemical Property of 2-<3-phenylacetamido-4-(m-acetamido)phenylthiocarbonate-(3R,4R)-azetidin-2-on-1-yl>-trichloroethyl acetate

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Technology Process of 2-<3-phenylacetamido-4-(m-acetamido)phenylthiocarbonate-(3R,4R)-azetidin-2-on-1-yl>-trichloroethyl acetate

There total 3 articles about 2-<3-phenylacetamido-4-(m-acetamido)phenylthiocarbonate-(3R,4R)-azetidin-2-on-1-yl>-trichloroethyl acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 122691-79-6
2-<3-phenylacetamido-4-thiochlorocarbonyl-(3R,4R)-azetidin-2-on-1-yl>-trichloroethyl acetate

: 621-42-1
meta-hydroxyacetanilide

: 122691-94-5
2-<3-phenylacetamido-4-(m-acetamido)phenylthiocarbonate-(3R,4R)-azetidin-2-on-1-yl>-trichloroethyl acetate

Guidance literature:: With triethylamine; In dichloromethane; at 20 ℃; for 2h; Yield given;
DOI:10.1016/0223-5234(88)90100-6

Reference yield:

: 87996-82-5
2-<3-benzyl-6-oxo-2-thia-4,7-diaza-(1R,5R)-bicyclo-<3.2.0>-hept-3-en-7-yl>-acetic acid-β-trichloroethyl ester

: 122691-94-5
2-<3-phenylacetamido-4-(m-acetamido)phenylthiocarbonate-(3R,4R)-azetidin-2-on-1-yl>-trichloroethyl acetate

Guidance literature:: Multi-step reaction with 3 steps

1: 80 percent / 1.2 N aq HCl / dimethylformamide / 1 h / Ambient temperature

2: 85 percent / triethylamine / toluene; CH₂Cl₂ / Ambient temperature

3: triethylamine / CH₂Cl₂ / 2 h / 20 °C

With hydrogenchloride; triethylamine; In dichloromethane; N,N-dimethyl-formamide; toluene;
DOI:10.1016/0223-5234(88)90100-6

Reference yield:

: 122691-74-1
2-<3-phenylacetamido-4-thiol-(3R,4R)-azetidin-2-on-1-yl>-trichloroethyl acetate

: 122691-94-5
2-<3-phenylacetamido-4-(m-acetamido)phenylthiocarbonate-(3R,4R)-azetidin-2-on-1-yl>-trichloroethyl acetate

Guidance literature:: Multi-step reaction with 2 steps

1: 85 percent / triethylamine / toluene; CH₂Cl₂ / Ambient temperature

2: triethylamine / CH₂Cl₂ / 2 h / 20 °C

With triethylamine; In dichloromethane; toluene;
DOI:10.1016/0223-5234(88)90100-6