2-C-(6-iodo-2,3-di-O-benzyl-4-azido-4,6-dideoxy-α-D-galactopyranosyl)acetone

Base Information

Chemical Name:2-C-(6-iodo-2,3-di-O-benzyl-4-azido-4,6-dideoxy-α-D-galactopyranosyl)acetone
CAS No.:1422964-64-4
Molecular Formula:C₂₃H₂₆IN₃O₄
Molecular Weight:535.382
Hs Code.:

Synonyms:2-C-(6-iodo-2,3-di-O-benzyl-4-azido-4,6-dideoxy-α-D-galactopyranosyl)acetone

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Chemical Property of 2-C-(6-iodo-2,3-di-O-benzyl-4-azido-4,6-dideoxy-α-D-galactopyranosyl)acetone

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Technology Process of 2-C-(6-iodo-2,3-di-O-benzyl-4-azido-4,6-dideoxy-α-D-galactopyranosyl)acetone

There total 5 articles about 2-C-(6-iodo-2,3-di-O-benzyl-4-azido-4,6-dideoxy-α-D-galactopyranosyl)acetone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

: 1422964-65-5
C₂₄H₂₉N₃O₇S

: 1422964-64-4
2-C-(6-iodo-2,3-di-O-benzyl-4-azido-4,6-dideoxy-α-D-galactopyranosyl)acetone

Guidance literature:: With potassium iodide; In N,N-dimethyl-formamide; at 80 ℃;
DOI:10.1021/jo3024973

Reference yield:

: 88714-23-2
C₂₄H₂₇N₃O₇

: 1422964-64-4
2-C-(6-iodo-2,3-di-O-benzyl-4-azido-4,6-dideoxy-α-D-galactopyranosyl)acetone

Guidance literature:: Multi-step reaction with 4 steps

1: trimethylsilyl trifluoromethanesulfonate / acetonitrile

2: palladium dichloride; copper dichloride / N,N-dimethyl-formamide; water

3: sodium methylate / methanol

4: potassium iodide / N,N-dimethyl-formamide / 80 °C

With trimethylsilyl trifluoromethanesulfonate; sodium methylate; potassium iodide; copper dichloride; palladium dichloride; In methanol; water; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1021/jo3024973

Reference yield:

: C₂₅H₂₉N₃O₆

: 1422964-64-4
2-C-(6-iodo-2,3-di-O-benzyl-4-azido-4,6-dideoxy-α-D-galactopyranosyl)acetone

Guidance literature:: Multi-step reaction with 2 steps

1: sodium methylate / methanol

2: potassium iodide / N,N-dimethyl-formamide / 80 °C

With sodium methylate; potassium iodide; In methanol; N,N-dimethyl-formamide;
DOI:10.1021/jo3024973