1-(4-methoxyphenylsulfonyl)-2-indolyl 1-methyl-4-hydroxy-4-piperidyl ketone

Base Information

• Chemical Name: 1-(4-methoxyphenylsulfonyl)-2-indolyl 1-methyl-4-hydroxy-4-piperidyl ketone
• CAS No.: 128721-25-5
• Molecular Formula: C₂₂H₂₄N₂O₅S
• Molecular Weight: 428.509

Synonyms:1-(4-methoxyphenylsulfonyl)-2-indolyl 1-methyl-4-hydroxy-4-piperidyl ketone

Chemical Property of 1-(4-methoxyphenylsulfonyl)-2-indolyl 1-methyl-4-hydroxy-4-piperidyl ketone

Chemical Property:

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Technology Process of 1-(4-methoxyphenylsulfonyl)-2-indolyl 1-methyl-4-hydroxy-4-piperidyl ketone

There total 9 articles about 1-(4-methoxyphenylsulfonyl)-2-indolyl 1-methyl-4-hydroxy-4-piperidyl ketone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

4-{Dimethoxy-[1-(4-methoxy-benzenesulfonyl)-1H-indol-2-yl]-methyl}-1-methyl-piperidin-4-ol (128721-44-8) → 1-(4-methoxyphenylsulfonyl)-2-indolyl 1-methyl-4-hydroxy-4-piperidyl ketone (128721-25-5)

Guidance literature:

With hydrogenchloride; In methanol; for 6h; Heating;

DOI:10.3987/COM-89-5240

Reference yield: 49.0%

1-methyl-4-<2-<1-(4-methoxyphenylsulfonyl)-2-indolyl>-1,3-dithian-2-yl>-4-piperidinol (128721-21-1) → 1-(4-methoxyphenylsulfonyl)-2-indolyl 1-methyl-4-hydroxy-4-piperidyl ketone (128721-25-5)

Guidance literature:

With bis-[(trifluoroacetoxy)iodo]benzene; In water; acetonitrile; for 0.75h; Ambient temperature;

DOI:10.3987/COM-89-5240

Reference yield: 23.0%

4-{2-[1-(4-Methoxy-benzenesulfonyl)-1H-indol-2-yl]-1-oxo-1λ4-[1,3]dithian-2-yl}-1-methyl-piperidin-4-ol (128721-26-6) → 1-(4-methoxyphenylsulfonyl)-2-indolyl 1-methyl-4-hydroxy-4-piperidyl ketone (128721-25-5)

Guidance literature:

With acetic acid; at 65 ℃;

DOI:10.3987/COM-89-5240

upstream raw materials:

4-{Dimethoxy-[1-(4-methoxy-benzenesulfonyl)-1H-indol-2-yl]-methyl}-1-methyl-piperidin-4-ol

1-methyl-4-<2-<1-(4-methoxyphenylsulfonyl)-2-indolyl>-1,3-dithian-2-yl>-4-piperidinol

4-{2-[1-(4-Methoxy-benzenesulfonyl)-1H-indol-2-yl]-1-oxo-1λ⁴-[1,3]dithian-2-yl}-1-methyl-piperidin-4-ol

1-Methyl-4-piperidone

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