6-<<(benzamidomethyl)thio>methyl>-4-hydroxy-2-methoxy-4-methyl-3,4,5,6-tetrahydro-2H-pyran

Base Information

Chemical Name:6-<<(benzamidomethyl)thio>methyl>-4-hydroxy-2-methoxy-4-methyl-3,4,5,6-tetrahydro-2H-pyran
CAS No.:96228-42-1
Molecular Formula:C₁₆H₂₃NO₄S
Molecular Weight:325.429
Hs Code.:

Synonyms:6-<<(benzamidomethyl)thio>methyl>-4-hydroxy-2-methoxy-4-methyl-3,4,5,6-tetrahydro-2H-pyran

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Chemical Property of 6-<<(benzamidomethyl)thio>methyl>-4-hydroxy-2-methoxy-4-methyl-3,4,5,6-tetrahydro-2H-pyran

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Technology Process of 6-<<(benzamidomethyl)thio>methyl>-4-hydroxy-2-methoxy-4-methyl-3,4,5,6-tetrahydro-2H-pyran

There total 5 articles about 6-<<(benzamidomethyl)thio>methyl>-4-hydroxy-2-methoxy-4-methyl-3,4,5,6-tetrahydro-2H-pyran which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 96228-40-9,96228-41-0
1-<(benzamidomethyl)thio>-6,6-dimethoxy-4-methyl-2,4-hexanediol

: 96228-42-1
6-<<(benzamidomethyl)thio>methyl>-4-hydroxy-2-methoxy-4-methyl-3,4,5,6-tetrahydro-2H-pyran

Guidance literature:: With sulfuric acid; In methanol; acetone; for 44h;
DOI:10.1021/jo00212a002

Reference yield:

: 38221-33-9
N-<(diethylamino)methyl>benzamide

: 96228-42-1
6-<<(benzamidomethyl)thio>methyl>-4-hydroxy-2-methoxy-4-methyl-3,4,5,6-tetrahydro-2H-pyran

Guidance literature:: Multi-step reaction with 2 steps

1: 44.8 percent / NaOH, / benzene / 1.) reflux, 4 h, 2.) RT, overnight,

2: 90 percent / H₂SO₄ / acetone; methanol / 44 h

With sodium hydroxide; sulfuric acid; In methanol; acetone; benzene;
DOI:10.1021/jo00212a002

Reference yield:

: 138832-35-6
1,1-dimethoxy-3-methyl-5-hexene-3-ol

: 96228-42-1
6-<<(benzamidomethyl)thio>methyl>-4-hydroxy-2-methoxy-4-methyl-3,4,5,6-tetrahydro-2H-pyran

Guidance literature:: Multi-step reaction with 4 steps

1: 69 percent / m-chloroperbenzoic acid (85percent) / CHCl₃ / 64 h / Ambient temperature

2: 81 percent / NaOH, H₂S / methanol / 17 h / Ambient temperature

3: 44.8 percent / NaOH, / benzene / 1.) reflux, 4 h, 2.) RT, overnight,

4: 90 percent / H₂SO₄ / acetone; methanol / 44 h

With sodium hydroxide; sulfuric acid; hydrogen sulfide; 3-chloro-benzenecarboperoxoic acid; In methanol; chloroform; acetone; benzene;
DOI:10.1021/jo00212a002