(2S,3R)-3-[(4S,5R)-5-((R)-1-Hydroxy-2-trityloxy-ethyl)-2,2-dimethyl-[1,3]dioxolan-4-yl]-oxirane-2-carboxylic acid diethylamide

Base Information

Chemical Name:(2S,3R)-3-[(4S,5R)-5-((R)-1-Hydroxy-2-trityloxy-ethyl)-2,2-dimethyl-[1,3]dioxolan-4-yl]-oxirane-2-carboxylic acid diethylamide
CAS No.:180591-23-5
Molecular Formula:C₃₃H₃₉NO₆
Molecular Weight:545.676
Hs Code.:

Synonyms:(2S,3R)-3-[(4S,5R)-5-((R)-1-Hydroxy-2-trityloxy-ethyl)-2,2-dimethyl-[1,3]dioxolan-4-yl]-oxirane-2-carboxylic acid diethylamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (2S,3R)-3-[(4S,5R)-5-((R)-1-Hydroxy-2-trityloxy-ethyl)-2,2-dimethyl-[1,3]dioxolan-4-yl]-oxirane-2-carboxylic acid diethylamide

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Technology Process of (2S,3R)-3-[(4S,5R)-5-((R)-1-Hydroxy-2-trityloxy-ethyl)-2,2-dimethyl-[1,3]dioxolan-4-yl]-oxirane-2-carboxylic acid diethylamide

There total 2 articles about (2S,3R)-3-[(4S,5R)-5-((R)-1-Hydroxy-2-trityloxy-ethyl)-2,2-dimethyl-[1,3]dioxolan-4-yl]-oxirane-2-carboxylic acid diethylamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 40.0%

: 688321-37-1
N,N-diethyl 2,3-anhydro-4,5-O-isopropylidene-7-O-trityl-D-altro-6-heptulosamide

: N,N-diethyl 3,6-dideoxy-3,6-imino-4,5-O-isopropylidene-7-O-trityl-D-glycero-D-manno-heptonamide

: N,N-diethyl-2-hydroxy-2-(6-hydroxy-2,2-dimethyl-6-trityloxymethyl-tetrahydro-furo[3,4-d][1,3]dioxol-4-yl)-acetamide

: 180591-23-5
(2S,3R)-3-[(4S,5R)-5-((R)-1-Hydroxy-2-trityloxy-ethyl)-2,2-dimethyl-[1,3]dioxolan-4-yl]-oxirane-2-carboxylic acid diethylamide

Guidance literature:: With molecular sieve; ammonium formate; sodium cyanoborohydride; In methanol; for 11h;
DOI:10.1016/j.tetasy.2004.11.054

Reference yield:

: 688321-37-1
N,N-diethyl 2,3-anhydro-4,5-O-isopropylidene-7-O-trityl-D-altro-6-heptulosamide

: (2S,3R)-3-[(4S,5R)-5-((S)-1-Hydroxy-2-trityloxy-ethyl)-2,2-dimethyl-[1,3]dioxolan-4-yl]-oxirane-2-carboxylic acid diethylamide

: 180591-23-5
(2S,3R)-3-[(4S,5R)-5-((R)-1-Hydroxy-2-trityloxy-ethyl)-2,2-dimethyl-[1,3]dioxolan-4-yl]-oxirane-2-carboxylic acid diethylamide

Guidance literature:: With sodium tetrahydroborate; In ethanol; at 0 ℃; for 0.25h; Title compound not separated from byproducts;
DOI:10.1016/j.tetasy.2004.11.054