3,5-dinitro-4-[N'-phenyl-N'-[p-(4'-formyl-2',6'-dinitrophenyl)phenylamino]hydrazinyl]benzaldehyde

Base Information

Chemical Name:3,5-dinitro-4-[N'-phenyl-N'-[p-(4'-formyl-2',6'-dinitrophenyl)phenylamino]hydrazinyl]benzaldehyde
CAS No.:1478732-76-1
Molecular Formula:C₂₆H₁₇N₇O₁₀
Molecular Weight:587.462
Hs Code.:

Synonyms:3,5-dinitro-4-[N'-phenyl-N'-[p-(4'-formyl-2',6'-dinitrophenyl)phenylamino]hydrazinyl]benzaldehyde

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Chemical Property of 3,5-dinitro-4-[N'-phenyl-N'-[p-(4'-formyl-2',6'-dinitrophenyl)phenylamino]hydrazinyl]benzaldehyde

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Technology Process of 3,5-dinitro-4-[N'-phenyl-N'-[p-(4'-formyl-2',6'-dinitrophenyl)phenylamino]hydrazinyl]benzaldehyde

There total 6 articles about 3,5-dinitro-4-[N'-phenyl-N'-[p-(4'-formyl-2',6'-dinitrophenyl)phenylamino]hydrazinyl]benzaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 35.0%

: 3,5-dinitro-4-[N'-phenyl-N'-[p-(4'-cyano-2',6'-dinitrophenyl)phenylamino]hydrazinyl]benzonitrile

: 1478732-76-1
3,5-dinitro-4-[N'-phenyl-N'-[p-(4'-formyl-2',6'-dinitrophenyl)phenylamino]hydrazinyl]benzaldehyde

Guidance literature:: With diisobutylaluminium hydride; In dichloromethane; at -78 - 20 ℃; for 1h; Cooling with acetone-dry ice;
DOI:10.3998/ark.5550190.p008.314

Reference yield:

: 1930-72-9
4-chloro-3,5-dinitrobenzonitrile

: 1478732-76-1
3,5-dinitro-4-[N'-phenyl-N'-[p-(4'-formyl-2',6'-dinitrophenyl)phenylamino]hydrazinyl]benzaldehyde

Guidance literature:: Multi-step reaction with 4 steps

1: sodium hydrogencarbonate / ethanol / 2 h / Reflux

2: sodium sulfate; lead dioxide / dichloromethane / 6 h

3: ascorbic acid / dichloromethane; water

4: diisobutylaluminium hydride / dichloromethane / 1 h / -78 - 20 °C / Cooling with acetone-dry ice

With diisobutylaluminium hydride; sodium hydrogencarbonate; lead dioxide; sodium sulfate; ascorbic acid; In ethanol; dichloromethane; water;
DOI:10.3998/ark.5550190.p008.314

Reference yield:

: 530-47-2,29666-92-0
N,N-diphenylhydrazine hydrochloride

: 1478732-76-1
3,5-dinitro-4-[N'-phenyl-N'-[p-(4'-formyl-2',6'-dinitrophenyl)phenylamino]hydrazinyl]benzaldehyde

Guidance literature:: Multi-step reaction with 4 steps

1: sodium hydrogencarbonate / ethanol / 2 h / Reflux

2: sodium sulfate; lead dioxide / dichloromethane / 6 h

3: ascorbic acid / dichloromethane; water

4: diisobutylaluminium hydride / dichloromethane / 1 h / -78 - 20 °C / Cooling with acetone-dry ice

With diisobutylaluminium hydride; sodium hydrogencarbonate; lead dioxide; sodium sulfate; ascorbic acid; In ethanol; dichloromethane; water;
DOI:10.3998/ark.5550190.p008.314