methyl (2E,6E)-8-[t-butyl(diphenyl)silyl]oxy-2,6-dimethyl-2,6-octadienoate

Base Information

Chemical Name:methyl (2E,6E)-8-[t-butyl(diphenyl)silyl]oxy-2,6-dimethyl-2,6-octadienoate
CAS No.:916754-48-8
Molecular Formula:C₂₇H₃₆O₃Si
Molecular Weight:436.667
Hs Code.:

Synonyms:methyl (2E,6E)-8-[t-butyl(diphenyl)silyl]oxy-2,6-dimethyl-2,6-octadienoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of methyl (2E,6E)-8-[t-butyl(diphenyl)silyl]oxy-2,6-dimethyl-2,6-octadienoate

Chemical Property:

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Technology Process of methyl (2E,6E)-8-[t-butyl(diphenyl)silyl]oxy-2,6-dimethyl-2,6-octadienoate

There total 5 articles about methyl (2E,6E)-8-[t-butyl(diphenyl)silyl]oxy-2,6-dimethyl-2,6-octadienoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 106-24-1
Geraniol

: 916754-48-8
methyl (2E,6E)-8-[t-butyl(diphenyl)silyl]oxy-2,6-dimethyl-2,6-octadienoate

Guidance literature:: Multi-step reaction with 4 steps

1: 100 percent / imidazole / dimethylformamide / 1 h / 20 °C

2: 70 percent / MCPBA / CHCl₃ / 1 h / 0 °C

3: HIO₄*2H₂O / tetrahydrofuran; diethyl ether / 1 h / 0 °C

4: 7.0 g / CH₂Cl₂ / 3 h / 20 °C

With 1H-imidazole; periodic acid; 3-chloro-benzenecarboperoxoic acid; In tetrahydrofuran; diethyl ether; dichloromethane; chloroform; N,N-dimethyl-formamide;
DOI:10.1002/ejoc.200600367

Reference yield:

: 139109-03-8,117638-12-7
tert-butyl ({[(2E)-3,7-dimethylocta-2,6-dien-1-yl]oxy})diphenylsilane

: 916754-48-8
methyl (2E,6E)-8-[t-butyl(diphenyl)silyl]oxy-2,6-dimethyl-2,6-octadienoate

Guidance literature:: Multi-step reaction with 3 steps

1: 70 percent / MCPBA / CHCl₃ / 1 h / 0 °C

2: HIO₄*2H₂O / tetrahydrofuran; diethyl ether / 1 h / 0 °C

3: 7.0 g / CH₂Cl₂ / 3 h / 20 °C

With periodic acid; 3-chloro-benzenecarboperoxoic acid; In tetrahydrofuran; diethyl ether; dichloromethane; chloroform;
DOI:10.1002/ejoc.200600367

Reference yield:

: 58479-61-1
tert-butylchlorodiphenylsilane

: 916754-48-8
methyl (2E,6E)-8-[t-butyl(diphenyl)silyl]oxy-2,6-dimethyl-2,6-octadienoate

Guidance literature:: Multi-step reaction with 4 steps

1: 100 percent / imidazole / dimethylformamide / 1 h / 20 °C

2: 70 percent / MCPBA / CHCl₃ / 1 h / 0 °C

3: HIO₄*2H₂O / tetrahydrofuran; diethyl ether / 1 h / 0 °C

4: 7.0 g / CH₂Cl₂ / 3 h / 20 °C

With 1H-imidazole; periodic acid; 3-chloro-benzenecarboperoxoic acid; In tetrahydrofuran; diethyl ether; dichloromethane; chloroform; N,N-dimethyl-formamide;
DOI:10.1002/ejoc.200600367