benzyl 9-methoxy-2-oxo-5-phenyl-2,3-dihydro-1H-benzo[e][1,4]diazepin-3-ylcarbamate

Base Information

Chemical Name:benzyl 9-methoxy-2-oxo-5-phenyl-2,3-dihydro-1H-benzo[e][1,4]diazepin-3-ylcarbamate
CAS No.:1582184-79-9
Molecular Formula:C₂₄H₂₁N₃O₄
Molecular Weight:415.448
Hs Code.:

Synonyms:benzyl 9-methoxy-2-oxo-5-phenyl-2,3-dihydro-1H-benzo[e][1,4]diazepin-3-ylcarbamate

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Chemical Property of benzyl 9-methoxy-2-oxo-5-phenyl-2,3-dihydro-1H-benzo[e][1,4]diazepin-3-ylcarbamate

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Technology Process of benzyl 9-methoxy-2-oxo-5-phenyl-2,3-dihydro-1H-benzo[e][1,4]diazepin-3-ylcarbamate

There total 4 articles about benzyl 9-methoxy-2-oxo-5-phenyl-2,3-dihydro-1H-benzo[e][1,4]diazepin-3-ylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: (2-amino-3-methoxyphenyl)(phenyl)methanone

: 517874-18-9
(Benzotriazol-1-yl-chlorocarbonyl-methyl)-carbamic acid benzyl ester

: 1582184-79-9
benzyl 9-methoxy-2-oxo-5-phenyl-2,3-dihydro-1H-benzo[e][1,4]diazepin-3-ylcarbamate

Guidance literature:: (2-amino-3-methoxyphenyl)(phenyl)methanone; (Benzotriazol-1-yl-chlorocarbonyl-methyl)-carbamic acid benzyl ester; With triethylamine; In dichloromethane; at 0 - 20 ℃; for 1.91667h;

With ammonia; In methanol; for 16h;

With acetic acid; In methanol; for 5h;

Reference yield:

: 3177-80-8
2-amino-3-methoxybenzoic acid

: 1582184-79-9
benzyl 9-methoxy-2-oxo-5-phenyl-2,3-dihydro-1H-benzo[e][1,4]diazepin-3-ylcarbamate

Guidance literature:: Multi-step reaction with 3 steps

1.1: 3 h / 140 °C

2.1: tetrahydrofuran; toluene; diethyl ether / 0 - 20 °C

2.2: 100 °C

3.1: triethylamine / dichloromethane / 1.92 h / 0 - 20 °C

3.2: 16 h

3.3: 5 h

With triethylamine; In tetrahydrofuran; diethyl ether; dichloromethane; toluene;

Reference yield:

: 54905-94-1
8-methoxy-2-methyl-4H-benzo[d][1,3]oxazin-4-one

: 1582184-79-9
benzyl 9-methoxy-2-oxo-5-phenyl-2,3-dihydro-1H-benzo[e][1,4]diazepin-3-ylcarbamate

Guidance literature:: Multi-step reaction with 2 steps

1.1: tetrahydrofuran; toluene; diethyl ether / 0 - 20 °C

1.2: 100 °C

2.1: triethylamine / dichloromethane / 1.92 h / 0 - 20 °C

2.2: 16 h

2.3: 5 h

With triethylamine; In tetrahydrofuran; diethyl ether; dichloromethane; toluene;