(S)-2-((1-amino-1-oxo-3-phenylpropan-2-ylamino)methyl)-5-methoxy-3-(4-nitrophenoxy)phenyl acetate

Base Information

• Chemical Name: (S)-2-((1-amino-1-oxo-3-phenylpropan-2-ylamino)methyl)-5-methoxy-3-(4-nitrophenoxy)phenyl acetate
• CAS No.: 1078141-18-0
• Molecular Formula: C₂₅H₂₅N₃O₇
• Molecular Weight: 479.489

Synonyms:(S)-2-((1-amino-1-oxo-3-phenylpropan-2-ylamino)methyl)-5-methoxy-3-(4-nitrophenoxy)phenyl acetate

Chemical Property of (S)-2-((1-amino-1-oxo-3-phenylpropan-2-ylamino)methyl)-5-methoxy-3-(4-nitrophenoxy)phenyl acetate

Chemical Property:

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Technology Process of (S)-2-((1-amino-1-oxo-3-phenylpropan-2-ylamino)methyl)-5-methoxy-3-(4-nitrophenoxy)phenyl acetate

There total 1 articles about (S)-2-((1-amino-1-oxo-3-phenylpropan-2-ylamino)methyl)-5-methoxy-3-(4-nitrophenoxy)phenyl acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 31.0%

2-formyl-5-methoxy-3-(4-nitrophenoxy)phenyl acetate (1078141-16-8) + L-Phenylalanine amide (5241-58-7) → (S)-2-((1-amino-1-oxo-3-phenylpropan-2-ylamino)methyl)-5-methoxy-3-(4-nitrophenoxy)phenyl acetate (1078141-18-0)

Guidance literature:

With sodium tris(acetoxy)borohydride; acetic acid; In tetrahydrofuran; dichloromethane; at 20 ℃; for 15h;

DOI:10.1016/j.tet.2008.08.037

Reference yield: 54.0%

(S)-2-((1-amino-1-oxo-3-phenylpropan-2-ylamino)methyl)-5-methoxy-3-(4-nitrophenoxy)phenyl acetate (1078141-18-0) → (S)-2-((1-amino-1-oxo-3-phenylpropan-2-ylamino)methyl)-3-(4-aminophenoxy)-5-methoxyphenyl acetate (1078141-20-4)

Guidance literature:

With hydrogen; platinum(IV) oxide; In ethyl acetate; at 20 ℃; for 15h;

DOI:10.1016/j.tet.2008.08.037

upstream raw materials:

2-formyl-5-methoxy-3-(4-nitrophenoxy)phenyl acetate

L-Phenylalanine amide

Downstream raw materials:

(S)-2-((1-amino-1-oxo-3-phenylpropan-2-ylamino)methyl)-3-(4-aminophenoxy)-5-methoxyphenyl acetate

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