1D-(1,2,4,5/3)-1,5-di-O-benzoyl-2,3-di-O-benzyl-1,2,3,4,5-cyclohexanepentol

Base Information

• Chemical Name: 1D-(1,2,4,5/3)-1,5-di-O-benzoyl-2,3-di-O-benzyl-1,2,3,4,5-cyclohexanepentol
• CAS No.: 1197981-63-7
• Molecular Formula: C₃₄H₃₂O₇
• Molecular Weight: 552.624

Synonyms:1D-(1,2,4,5/3)-1,5-di-O-benzoyl-2,3-di-O-benzyl-1,2,3,4,5-cyclohexanepentol

Chemical Property of 1D-(1,2,4,5/3)-1,5-di-O-benzoyl-2,3-di-O-benzyl-1,2,3,4,5-cyclohexanepentol

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Technology Process of 1D-(1,2,4,5/3)-1,5-di-O-benzoyl-2,3-di-O-benzyl-1,2,3,4,5-cyclohexanepentol

There total 1 articles about 1D-(1,2,4,5/3)-1,5-di-O-benzoyl-2,3-di-O-benzyl-1,2,3,4,5-cyclohexanepentol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C37H36O7 → 1D-(1,2,4,5/3)-1,5-di-O-benzoyl-2,3-di-O-benzyl-1,2,3,4,5-cyclohexanepentol (1197981-63-7)

Guidance literature:

With methanol; palladium dichloride; at 20 ℃; for 2h; Inert atmosphere;

DOI:10.1039/b907518f

Reference yield: 56.0%

1D-(1,2,4,5/3)-1,5-di-O-benzoyl-2,3-di-O-benzyl-1,2,3,4,5-cyclohexanepentol (1197981-63-7) + 4-methoxyphenyl 2,2,2-trichloroacetimidate → 1D-(1,2,4,5/3)-1,5-di-O-benzoyl-2,3-di-O-benzyl-4-(4-methoxy)benzyl-1,2,3,4,5-cyclohexanepentol

Guidance literature:

With boron trifluoride diethyl etherate; In hexane; dichloromethane; at 0 ℃; Inert atmosphere;

DOI:10.1039/b907518f

Reference yield:

C27H28N6O3S (1197981-91-1) + 1D-(1,2,4,5/3)-1,5-di-O-benzoyl-2,3-di-O-benzyl-1,2,3,4,5-cyclohexanepentol (1197981-63-7) → C54H52N6O10 (1197982-38-9)

Guidance literature:

C₂₇H₂₈N₆O₃S; 1D-(1,2,4,5/3)-1,5-di-O-benzoyl-2,3-di-O-benzyl-1,2,3,4,5-cyclohexanepentol; With N-iodo-succinimide; In dichloromethane; for 0.5h; Molecular sieve; Inert atmosphere;

With trifluorormethanesulfonic acid; In diethyl ether; dichloromethane; at -40 - -20 ℃; Inert atmosphere;

DOI:10.1039/b907518f

Downstream raw materials:

C₅₄H₅₂N₆O₁₀

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