C₂₃H₂₇O₄P

Base Information

• Chemical Name: C₂₃H₂₇O₄P
• CAS No.: 1384638-50-9
• Molecular Formula: C₂₃H₂₇O₄P
• Molecular Weight: 398.439
• Mol file: 1384638-50-9.mol

Synonyms:C₂₃H₂₇O₄P

Chemical Property of C₂₃H₂₇O₄P

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₂₃H₂₇O₄P

There total 4 articles about C₂₃H₂₇O₄P which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

C23H27O4P (1384638-30-5) → C23H27O4P (1384638-50-9)

Guidance literature:

With silver hexafluoroantimonate; (triphenylphosphine)gold(I) chloride; In 1,2-dichloro-ethane; at 70 ℃; for 3h;

DOI:10.1016/j.tetlet.2012.04.060

Reference yield:

phenylacetylene (536-74-3) → C23H27O4P (1384638-50-9)

Guidance literature:

Multi-step reaction with 3 steps

1: copper(l) iodide; diisopropylamine; triphenylphosphine; palladium dichloride / tetrahydrofuran / 0 °C

2: triethylamine / tetrahydrofuran / 2 h / 20 °C

3: (triphenylphosphine)gold(I) chloride; silver hexafluoroantimonate / 1,2-dichloro-ethane / 3 h / 70 °C

With silver hexafluoroantimonate; copper(l) iodide; (triphenylphosphine)gold(I) chloride; triethylamine; diisopropylamine; triphenylphosphine; palladium dichloride; In tetrahydrofuran; 1,2-dichloro-ethane; 1: Sonogashira coupling / 2: Pudovik reaction;

DOI:10.1016/j.tetlet.2012.04.060

Reference yield:

(Z)-2-iodo-3-phenylacrylaldehyde (116544-98-0) → C23H27O4P (1384638-50-9)

Guidance literature:

Multi-step reaction with 3 steps

1: copper(l) iodide; diisopropylamine; triphenylphosphine; palladium dichloride / tetrahydrofuran / 0 °C

2: triethylamine / tetrahydrofuran / 2 h / 20 °C

3: (triphenylphosphine)gold(I) chloride; silver hexafluoroantimonate / 1,2-dichloro-ethane / 3 h / 70 °C

With silver hexafluoroantimonate; copper(l) iodide; (triphenylphosphine)gold(I) chloride; triethylamine; diisopropylamine; triphenylphosphine; palladium dichloride; In tetrahydrofuran; 1,2-dichloro-ethane; 1: Sonogashira coupling / 2: Pudovik reaction;

DOI:10.1016/j.tetlet.2012.04.060

upstream raw materials:

C₂₃H₂₇O₄P

diisopropyl hydrogenphosphonate

(E)-2-phenylethynyl-3-phenylpropen-1-al

phenylacetylene