di-tert-butyl [3,3'-iminobis(5-tert-butyl-2-methoxyphenyl)]dicarbamate

Base Information

• Chemical Name: di-tert-butyl [3,3'-iminobis(5-tert-butyl-2-methoxyphenyl)]dicarbamate
• CAS No.: 1048983-39-6
• Molecular Formula: C₃₂H₄₉N₃O₆
• Molecular Weight: 571.758
• Mol file: 1048983-39-6.mol

Synonyms:di-tert-butyl [3,3'-iminobis(5-tert-butyl-2-methoxyphenyl)]dicarbamate

Chemical Property of di-tert-butyl [3,3'-iminobis(5-tert-butyl-2-methoxyphenyl)]dicarbamate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of di-tert-butyl [3,3'-iminobis(5-tert-butyl-2-methoxyphenyl)]dicarbamate

There total 1 articles about di-tert-butyl [3,3'-iminobis(5-tert-butyl-2-methoxyphenyl)]dicarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

tert-butyl (3-amino-5-tert-butyl-2-methoxyphenyl)carbamate + tert-butyl (3-bromo-5-tert-butyl-2-methoxyphenyl)carbamate (1048983-38-5) → di-tert-butyl [3,3'-iminobis(5-tert-butyl-2-methoxyphenyl)]dicarbamate (1048983-39-6)

Guidance literature:

With bis[2-(diphenylphosphino)phenyl] ether; sodium t-butanolate; palladium diacetate; In toluene; at 80 ℃; for 23h;

DOI:10.1021/jo801543z

Reference yield:

di-tert-butyl [3,3'-iminobis(5-tert-butyl-2-methoxyphenyl)]dicarbamate (1048983-39-6) + di-tert-butyl dicarbonate (24424-99-5) → C42H65N3O10

Guidance literature:

With dmap; In tetrahydrofuran; for 15h; Heating;

DOI:10.1021/jo801543z

upstream raw materials:

tert-butyl (3-bromo-5-tert-butyl-2-methoxyphenyl)carbamate