C₂₂H₂₁NO₄

Base Information

Chemical Name:C₂₂H₂₁NO₄
CAS No.:1017280-72-6
Molecular Formula:C₂₂H₂₁NO₄
Molecular Weight:363.413
Hs Code.:

C<sub>22</sub>H<sub>21</sub>NO<sub>4</sub>

Synonyms:C₂₂H₂₁NO₄

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₂H₂₁NO₄

Chemical Property:

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Technology Process of C₂₂H₂₁NO₄

There total 4 articles about C₂₂H₂₁NO₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

: 1017280-67-9
C₂₁H₁₈ClNO₄

: 823-96-1
Trimethylboroxine

: 1017280-72-6
C₂₂H₂₁NO₄

Guidance literature:: With potassium carbonate; [1,3-bis(2,6-diisopropylphenyl)imidazol-2-ylidene](3-chloropyridyl)palladium(II) dichloride; In 1,4-dioxane; at 100 ℃; for 22h;
DOI:10.1021/ja7113486

Reference yield:

: 1017280-59-9
O₂N(Cl)C₆H₃C₆H₂(OBn)(OH)SnBu₃

: 1017280-72-6
C₂₂H₂₁NO₄

Guidance literature:: Multi-step reaction with 4 steps

1: sodium hydride / N,N-dimethyl-formamide

2: iodine / toluene

3: caesium carbonate / tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; tricyclohexylphosphine / 1,4-dioxane / 80 °C

4: potassium carbonate / [1,3-bis(2,6-diisopropylphenyl)imidazol-2-ylidene](3-chloropyridyl)palladium(ll) dichloride / 1,4-dioxane / 100 °C / Molecular sieve

With iodine; sodium hydride; potassium carbonate; caesium carbonate; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; [1,3-bis(2,6-diisopropylphenyl)imidazol-2-ylidene](3-chloropyridyl)palladium(ll) dichloride; tricyclohexylphosphine; In 1,4-dioxane; N,N-dimethyl-formamide; toluene;

Reference yield:

: 1017280-66-8
C₂₀H₁₅ClINO₄

: 1017280-72-6
C₂₂H₂₁NO₄

Guidance literature:: Multi-step reaction with 2 steps

1: caesium carbonate / tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; tricyclohexylphosphine / 1,4-dioxane / 80 °C

2: potassium carbonate / [1,3-bis(2,6-diisopropylphenyl)imidazol-2-ylidene](3-chloropyridyl)palladium(ll) dichloride / 1,4-dioxane / 100 °C / Molecular sieve

With potassium carbonate; caesium carbonate; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; [1,3-bis(2,6-diisopropylphenyl)imidazol-2-ylidene](3-chloropyridyl)palladium(ll) dichloride; tricyclohexylphosphine; In 1,4-dioxane;