6-(4-chlorobenzylthio)-5-cyanopicolinic acid

Base Information

Chemical Name:6-(4-chlorobenzylthio)-5-cyanopicolinic acid
CAS No.:1198296-57-9
Molecular Formula:C₁₄H₉ClN₂O₂S
Molecular Weight:304.757
Hs Code.:

Synonyms:6-(4-chlorobenzylthio)-5-cyanopicolinic acid

Suppliers and Price of 6-(4-chlorobenzylthio)-5-cyanopicolinic acid

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 6-(4-chlorobenzylthio)-5-cyanopicolinic acid

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 6-(4-chlorobenzylthio)-5-cyanopicolinic acid

There total 3 articles about 6-(4-chlorobenzylthio)-5-cyanopicolinic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 53234-56-3
6-chloro-5-cyano-pyridine-2-carboxylic acid

: 6258-66-8
(4-chlorophenyl)methanethiol

: 1198296-57-9
6-(4-chlorobenzylthio)-5-cyanopicolinic acid

Guidance literature:: 6-chloro-5-cyano-pyridine-2-carboxylic acid; (4-chlorophenyl)methanethiol; With caesium carbonate; In N,N-dimethyl-formamide; at 45 ℃; for 16h;

With hydrogenchloride; In water; pH=2;

Reference yield:

: 28900-10-9
2-chloro-6-methylnicotinonitrile

: 1198296-57-9
6-(4-chlorobenzylthio)-5-cyanopicolinic acid

Guidance literature:: Multi-step reaction with 3 steps

1.1: chromium(VI) oxide; sulfuric acid / 20 °C

1.2: 0 °C

2.1: trichlorophosphate / 0.5 h / Reflux

2.2: 0 °C

3.1: caesium carbonate / N,N-dimethyl-formamide / 16 h / 45 °C

3.2: pH 2

With chromium(VI) oxide; sulfuric acid; caesium carbonate; trichlorophosphate; In N,N-dimethyl-formamide;

Reference yield:

: 1312772-66-9
6-chloro-5-(aminocarbonyl)-2-picolinic acid

: 1198296-57-9
6-(4-chlorobenzylthio)-5-cyanopicolinic acid

Guidance literature:: Multi-step reaction with 2 steps

1.1: trichlorophosphate / 0.5 h / Reflux

1.2: 0 °C

2.1: caesium carbonate / N,N-dimethyl-formamide / 16 h / 45 °C

2.2: pH 2

With caesium carbonate; trichlorophosphate; In N,N-dimethyl-formamide;