3,4-methylenedioxy-5,4'-dimethoxy-3'-(S-Trt-N^α-Fmoc-L-Cys)amido-Z-stilbene

Base Information

Chemical Name:3,4-methylenedioxy-5,4'-dimethoxy-3'-(S-Trt-N^α-Fmoc-L-Cys)amido-Z-stilbene
CAS No.:501034-07-7
Molecular Formula:C₅₄H₄₆N₂O₇S
Molecular Weight:867.034
Hs Code.:

3,4-methylenedioxy-5,4'-dimethoxy-3'-(S-Trt-N<sup>α</sup>-Fmoc-L-Cys)amido-Z-stilbene

Synonyms:3,4-methylenedioxy-5,4'-dimethoxy-3'-(S-Trt-N^α-Fmoc-L-Cys)amido-Z-stilbene

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Chemical Property of 3,4-methylenedioxy-5,4'-dimethoxy-3'-(S-Trt-N^α-Fmoc-L-Cys)amido-Z-stilbene

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Technology Process of 3,4-methylenedioxy-5,4'-dimethoxy-3'-(S-Trt-N^α-Fmoc-L-Cys)amido-Z-stilbene

There total 5 articles about 3,4-methylenedioxy-5,4'-dimethoxy-3'-(S-Trt-N^α-Fmoc-L-Cys)amido-Z-stilbene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 103213-32-7,167015-11-4
N-(9-fluorenylmethoxycarbonyl)-S-trityl-L-cysteine

: 501033-98-3
2-Methoxy-5-[(Z)-2-(7-methoxy-benzo[1,3]dioxol-5-yl)-vinyl]-phenylamine

: 501034-07-7
3,4-methylenedioxy-5,4'-dimethoxy-3'-(S-Trt-N^α-Fmoc-L-Cys)amido-Z-stilbene

Guidance literature:: With N-ethyl-N,N-diisopropylamine; bromo-tris(1-pyrrolidinyl)phosphonium hexafluorophosphate; In dichloromethane; at 20 ℃; for 1h;
DOI:10.1021/jm020204l

Reference yield:

: 3,4-methylenedioxy-5-methoxybenzyltriphenylphosphonium bromide

: 501034-07-7
3,4-methylenedioxy-5,4'-dimethoxy-3'-(S-Trt-N^α-Fmoc-L-Cys)amido-Z-stilbene

Guidance literature:: Multi-step reaction with 3 steps

1.1: nBuLi / tetrahydrofuran / 4 h / 20 °C

1.2: 31 percent / tetrahydrofuran / 18 h

2.1: 77 percent / Zn; AcOH / 1.5 h

3.1: 85 percent / bromo-tris-pyrrolidino-phosphonium hexafluorophosphate; DIPEA / CH₂Cl₂ / 1 h / 20 °C

With n-butyllithium; acetic acid; N-ethyl-N,N-diisopropylamine; bromo-tris(1-pyrrolidinyl)phosphonium hexafluorophosphate; zinc; In tetrahydrofuran; dichloromethane;
DOI:10.1021/jm020204l

Reference yield:

: 31680-08-7
4-methoxy-3-nitrobenzaldehyde

: 501034-07-7
3,4-methylenedioxy-5,4'-dimethoxy-3'-(S-Trt-N^α-Fmoc-L-Cys)amido-Z-stilbene

Guidance literature:: Multi-step reaction with 3 steps

1.1: nBuLi / tetrahydrofuran / 4 h / 20 °C

1.2: 31 percent / tetrahydrofuran / 18 h

2.1: 77 percent / Zn; AcOH / 1.5 h

3.1: 85 percent / bromo-tris-pyrrolidino-phosphonium hexafluorophosphate; DIPEA / CH₂Cl₂ / 1 h / 20 °C

With n-butyllithium; acetic acid; N-ethyl-N,N-diisopropylamine; bromo-tris(1-pyrrolidinyl)phosphonium hexafluorophosphate; zinc; In tetrahydrofuran; dichloromethane;
DOI:10.1021/jm020204l