4,4-bis-tert-butoxycarbonyl-heptanedioic acid dipentachlorophenyl ester

Base Information

Chemical Name:4,4-bis-tert-butoxycarbonyl-heptanedioic acid dipentachlorophenyl ester
CAS No.:441310-29-8
Molecular Formula:C₂₉H₂₆Cl₁₀O₈
Molecular Weight:857.051
Hs Code.:

4,4-bis-<i>tert</i>-butoxycarbonyl-heptanedioic acid dipentachlorophenyl ester

Synonyms:4,4-bis-tert-butoxycarbonyl-heptanedioic acid dipentachlorophenyl ester

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Chemical Property of 4,4-bis-tert-butoxycarbonyl-heptanedioic acid dipentachlorophenyl ester

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Technology Process of 4,4-bis-tert-butoxycarbonyl-heptanedioic acid dipentachlorophenyl ester

There total 3 articles about 4,4-bis-tert-butoxycarbonyl-heptanedioic acid dipentachlorophenyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.8%

: 87-86-5,67471-28-7
Pentachlorophenol

: 312303-59-6
4,4-bis-tert-butoxycarbonyl-heptanedioic acid

: 441310-29-8
4,4-bis-tert-butoxycarbonyl-heptanedioic acid dipentachlorophenyl ester

Guidance literature:: With dicyclohexyl-carbodiimide; In ethyl acetate; at 20 ℃; for 3h;
DOI:10.1021/jo010661u

Reference yield:

: 541-16-2
t-butyl malonate

: 441310-29-8
4,4-bis-tert-butoxycarbonyl-heptanedioic acid dipentachlorophenyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 89.5 percent / NaH / tetrahydrofuran; various solvent(s) / 5 h / 20 °C

2: 65 percent / NaOH / H₂O; methanol / 8 h / 20 °C

3: 82.8 percent / dicyclohexylcarbodiimide / ethyl acetate / 3 h / 20 °C

With sodium hydroxide; sodium hydride; dicyclohexyl-carbodiimide; In tetrahydrofuran; methanol; water; ethyl acetate;
DOI:10.1021/jo010661u

Reference yield:

: 441310-28-7
4,4-bis-tert-butoxycarbonyl-heptanedioic acid dimethyl ester

: 441310-29-8
4,4-bis-tert-butoxycarbonyl-heptanedioic acid dipentachlorophenyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 65 percent / NaOH / H₂O; methanol / 8 h / 20 °C

2: 82.8 percent / dicyclohexylcarbodiimide / ethyl acetate / 3 h / 20 °C

With sodium hydroxide; dicyclohexyl-carbodiimide; In methanol; water; ethyl acetate;
DOI:10.1021/jo010661u