N-<2-nitro-5-(n-pentylamino)phenyl>-N-valeroyl<2'-(tert-butoxycarbonyl)biphenyl-4-yl>methylamine

Base Information

Chemical Name:N-<2-nitro-5-(n-pentylamino)phenyl>-N-valeroyl<2'-(tert-butoxycarbonyl)biphenyl-4-yl>methylamine
CAS No.:152627-95-7
Molecular Formula:C₃₄H₄₃N₃O₅
Molecular Weight:573.733
Hs Code.:

Synonyms:N-<2-nitro-5-(n-pentylamino)phenyl>-N-valeroyl<2'-(tert-butoxycarbonyl)biphenyl-4-yl>methylamine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-<2-nitro-5-(n-pentylamino)phenyl>-N-valeroyl<2'-(tert-butoxycarbonyl)biphenyl-4-yl>methylamine

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Technology Process of N-<2-nitro-5-(n-pentylamino)phenyl>-N-valeroyl<2'-(tert-butoxycarbonyl)biphenyl-4-yl>methylamine

There total 3 articles about N-<2-nitro-5-(n-pentylamino)phenyl>-N-valeroyl<2'-(tert-butoxycarbonyl)biphenyl-4-yl>methylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: 110-58-7
n-Pentylamine

: 133085-59-3
tert.butyl 4'-[N-(5-chloro-2-nitro-phenyl)-pentanoylaminomethyl]biphenyl-2-carboxylate

: 152627-95-7
N-<2-nitro-5-(n-pentylamino)phenyl>-N-valeroyl<2'-(tert-butoxycarbonyl)biphenyl-4-yl>methylamine

Guidance literature:: In diethylene glycol dimethyl ether; at 150 ℃; for 28h;
DOI:10.1021/jm00077a007

Reference yield:

: 114772-40-6
4'-bromomethyl-biphenyl-2-carboxylic acid tert-butyl ester

: 152627-95-7
N-<2-nitro-5-(n-pentylamino)phenyl>-N-valeroyl<2'-(tert-butoxycarbonyl)biphenyl-4-yl>methylamine

Guidance literature:: Multi-step reaction with 2 steps

1: NaH / dimethylformamide

2: 77 percent / bis-(2-methoxy-ethyl) ether / 28 h / 150 °C

With sodium hydride; In diethylene glycol dimethyl ether; N,N-dimethyl-formamide;
DOI:10.1021/jm00077a007

Reference yield:

: 2-(valeroylamino)-4-chloronitrobenzene

: 152627-95-7
N-<2-nitro-5-(n-pentylamino)phenyl>-N-valeroyl<2'-(tert-butoxycarbonyl)biphenyl-4-yl>methylamine

Guidance literature:: Multi-step reaction with 2 steps

1: NaH / dimethylformamide

2: 77 percent / bis-(2-methoxy-ethyl) ether / 28 h / 150 °C

With sodium hydride; In diethylene glycol dimethyl ether; N,N-dimethyl-formamide;
DOI:10.1021/jm00077a007