Methyl-6-O-acetyl-2,3-di-O-benzyl-4-O-trichloracetyl-α-D-glucopyranosid

Base Information

Chemical Name:Methyl-6-O-acetyl-2,3-di-O-benzyl-4-O-trichloracetyl-α-D-glucopyranosid
CAS No.:79705-88-7
Molecular Formula:C₂₅H₂₇Cl₃O₈
Molecular Weight:561.844
Hs Code.:

Synonyms:Methyl-6-O-acetyl-2,3-di-O-benzyl-4-O-trichloracetyl-α-D-glucopyranosid

Suppliers and Price of Methyl-6-O-acetyl-2,3-di-O-benzyl-4-O-trichloracetyl-α-D-glucopyranosid

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Methyl-6-O-acetyl-2,3-di-O-benzyl-4-O-trichloracetyl-α-D-glucopyranosid

Chemical Property:

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Technology Process of Methyl-6-O-acetyl-2,3-di-O-benzyl-4-O-trichloracetyl-α-D-glucopyranosid

There total 2 articles about Methyl-6-O-acetyl-2,3-di-O-benzyl-4-O-trichloracetyl-α-D-glucopyranosid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 20771-21-5,51842-23-0,51842-24-1,117561-20-3,125884-32-4,51842-22-9
methyl 2,3-di-O-benzyl-6-O-acetyl-α-D-glucopyranoside

: 4124-31-6
trichloroacetic acid anhydride

: 79705-88-7
Methyl-6-O-acetyl-2,3-di-O-benzyl-4-O-trichloracetyl-α-D-glucopyranosid

Guidance literature:: In pyridine; at -20 ℃; for 0.416667h;

Reference yield:

: 17791-36-5
methyl 2,3-di-O-benzyl-α-D-glucopyranoside

: 79705-88-7
Methyl-6-O-acetyl-2,3-di-O-benzyl-4-O-trichloracetyl-α-D-glucopyranosid

Guidance literature:: Multi-step reaction with 2 steps

1: 65 percent / CHCl₃ / 10 h

2: 99 percent / pyridine / 0.42 h / -20 °C

In pyridine; chloroform;

Reference yield:

: 79705-88-7
Methyl-6-O-acetyl-2,3-di-O-benzyl-4-O-trichloracetyl-α-D-glucopyranosid

: 77710-81-7
1,6-Di-O-acetyl-4-O-(6-O-acetyl-2,3-di-O-benzyl-α-D-glucopyranosyl)-2,3-di-O-benzyl-α-D-galactopyranose

Guidance literature:: Multi-step reaction with 5 steps

1: 82 percent / conc. H₂SO₄ / -20 °C

2: 94 percent / TiBr₄ / CH₂Cl₂; ethyl acetate / Ambient temperature

3: 1) Hg(CN)2, HgBr₂, molecular sieves 4 Angstroem / 1) CH₂Cl₂, r.t., 2) CH₂Cl₂, -20 deg C

4: CF₃COOH / 12 h

5: 48 percent / NH₃ / diethyl ether

With 4 A molecular sieve; sulfuric acid; ammonia; mercury(II) cyanide; titanium(IV) bromide; trifluoroacetic acid; mercury dibromide; In diethyl ether; dichloromethane; ethyl acetate;