C₃₉H₅₀O₇

Base Information

Chemical Name:C₃₉H₅₀O₇
CAS No.:1531627-40-3
Molecular Formula:C₃₉H₅₀O₇
Molecular Weight:630.822
Hs Code.:

C<sub>39</sub>H<sub>50</sub>O<sub>7</sub>

Synonyms:C₃₉H₅₀O₇

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Chemical Property of C₃₉H₅₀O₇

Chemical Property:

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Technology Process of C₃₉H₅₀O₇

There total 25 articles about C₃₉H₅₀O₇ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 1531627-38-9
C₄₂H₅₄O₇

: 1531627-40-3
C₃₉H₅₀O₇

Guidance literature:: With camphor-10-sulfonic acid; In acetone; for 96h;
DOI:10.1021/ol403441c

Reference yield:

: 1309113-14-1
(E)-tert-butyl[(6-{[(4-methoxybenzyl)oxy]methyl}-4,4-dimethylhepta-2,6-dien-1-yl)oxy]dimethylsilane

: 1531627-40-3
C₃₉H₅₀O₇

Guidance literature:: Multi-step reaction with 14 steps

1.1: 2,3-dicyano-5,6-dichloro-p-benzoquinone / dichloromethane / 20 °C

2.1: titanium(IV) isopropylate; tert.-butylhydroperoxide / dichloromethane / 20 h / -25 °C

2.2: Molecular sieve

3.1: lithium aluminium tetrahydride / tetrahydrofuran / 1 h

4.1: PPTA / dichloromethane / 2 h / 20 °C

4.2: -78 - 20 °C

5.1: dmap; sodium hydrogencarbonate / dichloromethane / 3 h / 0 °C

6.1: potassium hexamethylsilazane / tetrahydrofuran / 1 h / -78 °C

6.2: -78 - 20 °C

7.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 2 h / 20 °C

8.1: NMO; tetrapropylammonium perruthennate / dichloromethane / 3 h / -30 °C / Molecular sieve

8.2: 0.42 h / -90 - -70 °C

9.1: tetrapropylammonium perruthennate; magnesium bromide ethyl etherate / dichloromethane / 3 h / 0 °C

10.1: 2,3-dicyano-5,6-dichloro-p-benzoquinone / dichloromethane / 0.83 h / 0 °C / pH 7

11.1: lithium aluminium tetrahydride / tetrahydrofuran / 65 h / -70 °C

12.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 0.25 h

13.1: copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; triethylamine / 120 h / Darkness

14.1: camphor-10-sulfonic acid / acetone / 96 h

With titanium(IV) isopropylate; tert.-butylhydroperoxide; dmap; copper(l) iodide; lithium aluminium tetrahydride; tetrakis(triphenylphosphine) palladium⁽⁰⁾; tetrapropylammonium perruthennate; NMO; camphor-10-sulfonic acid; tetrabutyl ammonium fluoride; potassium hexamethylsilazane; sodium hydrogencarbonate; magnesium bromide ethyl etherate; triethylamine; 2,3-dicyano-5,6-dichloro-p-benzoquinone; In tetrahydrofuran; dichloromethane; acetone;
DOI:10.1021/ol403441c

Reference yield:

: 1309113-21-0
(R,E)-(2-{5-[(tert-butyldimethylsilyl)oxy]-2,2-dimethylpent-3-en-1-yl}oxiran-2-yl)methanol

: 1531627-40-3
C₃₉H₅₀O₇

Guidance literature:: Multi-step reaction with 12 steps

1.1: lithium aluminium tetrahydride / tetrahydrofuran / 1 h

2.1: PPTA / dichloromethane / 2 h / 20 °C

2.2: -78 - 20 °C

3.1: dmap; sodium hydrogencarbonate / dichloromethane / 3 h / 0 °C

4.1: potassium hexamethylsilazane / tetrahydrofuran / 1 h / -78 °C

4.2: -78 - 20 °C

5.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 2 h / 20 °C

6.1: NMO; tetrapropylammonium perruthennate / dichloromethane / 3 h / -30 °C / Molecular sieve

6.2: 0.42 h / -90 - -70 °C

7.1: tetrapropylammonium perruthennate; magnesium bromide ethyl etherate / dichloromethane / 3 h / 0 °C

8.1: 2,3-dicyano-5,6-dichloro-p-benzoquinone / dichloromethane / 0.83 h / 0 °C / pH 7

9.1: lithium aluminium tetrahydride / tetrahydrofuran / 65 h / -70 °C

10.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 0.25 h

11.1: copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; triethylamine / 120 h / Darkness

12.1: camphor-10-sulfonic acid / acetone / 96 h

With dmap; copper(l) iodide; lithium aluminium tetrahydride; tetrakis(triphenylphosphine) palladium⁽⁰⁾; tetrapropylammonium perruthennate; NMO; camphor-10-sulfonic acid; tetrabutyl ammonium fluoride; potassium hexamethylsilazane; sodium hydrogencarbonate; magnesium bromide ethyl etherate; triethylamine; 2,3-dicyano-5,6-dichloro-p-benzoquinone; In tetrahydrofuran; dichloromethane; acetone;
DOI:10.1021/ol403441c