2L-2,4,5/3-2,4-dibenzoyloxy-5-hydroxy-3-toluene-p-sulphonyloxycyclohexanone

Base Information

Chemical Name:2L-2,4,5/3-2,4-dibenzoyloxy-5-hydroxy-3-toluene-p-sulphonyloxycyclohexanone
CAS No.:95640-22-5
Molecular Formula:C₂₇H₂₄O₉S
Molecular Weight:524.548
Hs Code.:

Synonyms:2L-2,4,5/3-2,4-dibenzoyloxy-5-hydroxy-3-toluene-p-sulphonyloxycyclohexanone

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Chemical Property of 2L-2,4,5/3-2,4-dibenzoyloxy-5-hydroxy-3-toluene-p-sulphonyloxycyclohexanone

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Technology Process of 2L-2,4,5/3-2,4-dibenzoyloxy-5-hydroxy-3-toluene-p-sulphonyloxycyclohexanone

There total 3 articles about 2L-2,4,5/3-2,4-dibenzoyloxy-5-hydroxy-3-toluene-p-sulphonyloxycyclohexanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: methyl 2,4-di-O-benzoyl-6-deoxy-3-O-tosyl-α-D-xylo-hex-5-enopyranoside

: 95640-22-5
2L-2,4,5/3-2,4-dibenzoyloxy-5-hydroxy-3-toluene-p-sulphonyloxycyclohexanone

Guidance literature:: With sulfuric acid; mercury(II) sulfate; In 1,4-dioxane; water; at 60 - 80 ℃;
DOI:10.1016/S0008-6215(00)90774-2

Reference yield:

: 28538-12-7
methyl 4,6-O-benzylidene-2-O-benzoyl-3-O-p-tolylsulfonyl-α-D-glucopyranoside

: 95640-22-5
2L-2,4,5/3-2,4-dibenzoyloxy-5-hydroxy-3-toluene-p-sulphonyloxycyclohexanone

Guidance literature:: Multi-step reaction with 3 steps

1: 75 percent / N-bromosuccinimide, barium carbonate / CCl₄ / 2 h / Heating

2: 82 percent / silver fluoride / pyridine / Ambient temperature

3: 72 percent / sulfuric acid, mercury(II) sulfate / H₂O; dioxane / 60 - 80 °C

With N-Bromosuccinimide; sulfuric acid; silver fluoride; mercury(II) sulfate; barium carbonate; In 1,4-dioxane; pyridine; tetrachloromethane; water;
DOI:10.1016/S0008-6215(00)90774-2

Reference yield:

: 66649-78-3
methyl 2,4-di-O-benzoyl-6-bromo-6-deoxy-3-O-tosyl-α-D-glucopyranoside

: 95640-22-5
2L-2,4,5/3-2,4-dibenzoyloxy-5-hydroxy-3-toluene-p-sulphonyloxycyclohexanone

Guidance literature:: Multi-step reaction with 2 steps

1: 82 percent / silver fluoride / pyridine / Ambient temperature

2: 72 percent / sulfuric acid, mercury(II) sulfate / H₂O; dioxane / 60 - 80 °C

With sulfuric acid; silver fluoride; mercury(II) sulfate; In 1,4-dioxane; pyridine; water;
DOI:10.1016/S0008-6215(00)90774-2