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C17H14N4OS*ClH

Base Information
  • Chemical Name:C17H14N4OS*ClH
  • CAS No.:1312429-93-8
  • Molecular Formula:C17H14N4OS*ClH
  • Molecular Weight:358.851
  • Hs Code.:
C<sub>17</sub>H<sub>14</sub>N<sub>4</sub>OS*ClH

Synonyms:C17H14N4OS*ClH

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Chemical Property of C17H14N4OS*ClH
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Technology Process of C17H14N4OS*ClH

There total 3 articles about C17H14N4OS*ClH which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
With trifluoroacetic acid; In dichloromethane; at 20 ℃; for 4h;
Guidance literature:
Multi-step reaction with 6 steps
1.1: sodium hexamethyldisilazane / toluene; tetrahydrofuran / 1.17 h / -60 °C / Inert atmosphere
1.2: 2 h / 0 °C
2.1: potassium phosphate / tetrakis(triphenylphosphine) palladium(0) / 1,4-dioxane / 6 h / Reflux
3.1: hydrazine hydrate / 1-methyl-pyrrolidin-2-one / 7 h / 95 °C
4.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol / N,N-dimethyl-formamide / 4 h / 20 °C / Inert atmosphere
5.1: Burgess Reagent / 1,2-dimethoxyethane / 0.5 h / 110 °C / Microwave irradiation
6.1: trifluoroacetic acid / dichloromethane / 4 h / 20 °C
With potassium phosphate; Burgess Reagent; sodium hexamethyldisilazane; benzotriazol-1-ol; hydrazine hydrate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; trifluoroacetic acid; tetrakis(triphenylphosphine) palladium(0); In tetrahydrofuran; 1,4-dioxane; 1-methyl-pyrrolidin-2-one; 1,2-dimethoxyethane; dichloromethane; N,N-dimethyl-formamide; toluene;
Guidance literature:
Multi-step reaction with 2 steps
1: Burgess Reagent / 1,2-dimethoxyethane / 0.5 h / 110 °C / Microwave irradiation
2: trifluoroacetic acid / dichloromethane / 4 h / 20 °C
With Burgess Reagent; trifluoroacetic acid; In 1,2-dimethoxyethane; dichloromethane;
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