N-benzyl-2-{2'-[(benzyl-ethyl-carbamoyl)-methoxy]-biphenyl-2-yloxy}-N-ethyl-acetamide

Base Information

• Chemical Name: N-benzyl-2-{2'-[(benzyl-ethyl-carbamoyl)-methoxy]-biphenyl-2-yloxy}-N-ethyl-acetamide
• CAS No.: 944242-79-9
• Molecular Formula: C₃₄H₃₆N₂O₄
• Molecular Weight: 536.671
• Mol file: 944242-79-9.mol

Synonyms:N-benzyl-2-{2'-[(benzyl-ethyl-carbamoyl)-methoxy]-biphenyl-2-yloxy}-N-ethyl-acetamide

Chemical Property of N-benzyl-2-{2'-[(benzyl-ethyl-carbamoyl)-methoxy]-biphenyl-2-yloxy}-N-ethyl-acetamide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of N-benzyl-2-{2'-[(benzyl-ethyl-carbamoyl)-methoxy]-biphenyl-2-yloxy}-N-ethyl-acetamide

There total 1 articles about N-benzyl-2-{2'-[(benzyl-ethyl-carbamoyl)-methoxy]-biphenyl-2-yloxy}-N-ethyl-acetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

N-benzyl-2-chloro-N-ethylacetamide (73685-55-9) + 2,2'-dihydroxybiphenyl (1806-29-7) → N-benzyl-2-{2'-[(benzyl-ethyl-carbamoyl)-methoxy]-biphenyl-2-yloxy}-N-ethyl-acetamide (944242-79-9)

Guidance literature:

With potassium carbonate; In N,N-dimethyl-formamide; at 110 ℃; for 7h;

DOI:10.1016/j.saa.2006.08.019

Reference yield:

N-benzyl-2-{2'-[(benzyl-ethyl-carbamoyl)-methoxy]-biphenyl-2-yloxy}-N-ethyl-acetamide (944242-79-9) + ytterbium(III) picrate → Y(picrato)3(N-benzyl-2-(2'-[(benzyl-ethyl-carbamoyl)methoxy]biphenyl-2-yloxy)-N-ethylacetamide)

Guidance literature:

In ethanol; soln. of ligand in EtOH added dropwise to soln. of Y compd. (molar ratio1:1) in EtOH; stirred at room temp. for 5 h; filtered; ppt. washed with EtOH; dried in vac. over P2O5 for 48 h; elem.anal.;

DOI:10.1016/j.saa.2006.08.019

Reference yield:

N-benzyl-2-{2'-[(benzyl-ethyl-carbamoyl)-methoxy]-biphenyl-2-yloxy}-N-ethyl-acetamide (944242-79-9) + terbium(III) picrate → Tb(picrato)3(N-benzyl-2-(2'-[(benzyl-ethyl-carbamoyl)methoxy]biphenyl-2-yloxy)-N-ethylacetamide)

Guidance literature:

In ethanol; soln. of ligand in EtOH added dropwise to soln. of Tb compd. (molar ratio 1:1) in EtOH; stirred at room temp. for 5 h; filtered; ppt. washed with EtOH; dried in vac. over P2O5 for 48 h; elem.anal.;

DOI:10.1016/j.saa.2006.08.019

upstream raw materials:

N-benzyl-2-chloro-N-ethylacetamide

2,2'-dihydroxybiphenyl