o-tolylphosphonic acid bis(N,N-diethylamide)

Base Information

Chemical Name:o-tolylphosphonic acid bis(N,N-diethylamide)
CAS No.:5510-95-2
Molecular Formula:C₁₅H₂₇N₂OP
Molecular Weight:282.366
Hs Code.:

Synonyms:o-tolylphosphonic acid bis(N,N-diethylamide)

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of o-tolylphosphonic acid bis(N,N-diethylamide)

Chemical Property:

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Technology Process of o-tolylphosphonic acid bis(N,N-diethylamide)

There total 3 articles about o-tolylphosphonic acid bis(N,N-diethylamide) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 113544-73-3
N,N,N',N'-tetraethyl-P-(2-methylphenyl)phosphonous diamide

: 5510-95-2
o-tolylphosphonic acid bis(N,N-diethylamide)

Guidance literature:: With dihydrogen peroxide; In tetrahydrofuran; diethyl ether; at 20 ℃; Inert atmosphere; Schlenk technique;
DOI:10.1002/ejoc.201300344

Reference yield:

: 685-83-6
bis(diethylamino)chlorophosphine

: 5510-95-2
o-tolylphosphonic acid bis(N,N-diethylamide)

Guidance literature:: Multi-step reaction with 2 steps

1: magnesium / diethyl ether; tetrahydrofuran / 2 h / 0 °C / Inert atmosphere; Schlenk technique

2: dihydrogen peroxide / diethyl ether; tetrahydrofuran / 20 °C / Inert atmosphere; Schlenk technique

With dihydrogen peroxide; magnesium; In tetrahydrofuran; diethyl ether;
DOI:10.1002/ejoc.201300344

Reference yield:

: 95-46-5
2-methylphenyl bromide

: 5510-95-2
o-tolylphosphonic acid bis(N,N-diethylamide)

Guidance literature:: Multi-step reaction with 2 steps

1: magnesium / diethyl ether; tetrahydrofuran / 2 h / 0 °C / Inert atmosphere; Schlenk technique

2: dihydrogen peroxide / diethyl ether; tetrahydrofuran / 20 °C / Inert atmosphere; Schlenk technique

With dihydrogen peroxide; magnesium; In tetrahydrofuran; diethyl ether;
DOI:10.1002/ejoc.201300344