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Technology Process of Pd((C6H5)NCH(CH3)CC(CH3)NC6H5)2

Pd((C6H5)NCH(CH3)CC(CH3)NC6H5)2

Base Information
  • Chemical Name:Pd((C6H5)NCH(CH3)CC(CH3)NC6H5)2
  • CAS No.:1088447-13-5
  • Molecular Formula:C34H34N4Pd
  • Molecular Weight:605.091
  • Hs Code.:
Pd((C<sub>6</sub>H<sub>5</sub>)NCH(CH<sub>3</sub>)CC(CH<sub>3</sub>)NC<sub>6</sub>H<sub>5</sub>)2

Synonyms:Pd((C6H5)NCH(CH3)CC(CH3)NC6H5)2

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Chemical Property of Pd((C6H5)NCH(CH3)CC(CH3)NC6H5)2
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Technology Process of Pd((C6H5)NCH(CH3)CC(CH3)NC6H5)2

There total 1 articles about Pd((C6H5)NCH(CH3)CC(CH3)NC6H5)2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

bis(benzonitrile)palladium(II) dichloride
15617-18-2,39958-10-6,14220-64-5

bis(benzonitrile)palladium(II) dichloride

PhNC(Me)CH<sub>2</sub>C(Me)NPh

PhNC(Me)CH2C(Me)NPh

Pd((C<sub>6</sub>H<sub>5</sub>)NCH(CH<sub>3</sub>)CC(CH<sub>3</sub>)NC<sub>6</sub>H<sub>5</sub>)2
1088447-13-5

Pd((C6H5)NCH(CH3)CC(CH3)NC6H5)2

Guidance literature:
With LiO(t-C4H9); In tetrahydrofuran; byproducts: LiCl; soln. of palladium complex in THF was added to soln. of mixture of diimine and LiO(t)Bu in THF; after 2.5 h filtered through celite, filtrate was evad. in vac., extd. with pentane, filtered through celite, filtrate was evapd., elem. anal.;
DOI:10.1021/ic801557c

Reference yield: 65.0%

Pd((C<sub>6</sub>H<sub>5</sub>)NCH(CH<sub>3</sub>)CC(CH<sub>3</sub>)NC<sub>6</sub>H<sub>5</sub>)2
1088447-13-5

Pd((C6H5)NCH(CH3)CC(CH3)NC6H5)2

water
7732-18-5

water

Pd((C<sub>6</sub>H<sub>5</sub>)NCH(CH<sub>3</sub>)CC(CH<sub>3</sub>)O)2

Pd((C6H5)NCH(CH3)CC(CH3)O)2

Guidance literature:
In diethyl ether; byproducts: NH2C6H5; palladium complex was dissolved in nondried ether, kepk at ambient temp.overnight; crystals were separated, washed with cold ether, elem. anal.;
DOI:10.1021/ic801557c
upstream raw materials:

bis(benzonitrile)palladium(II) dichloride

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