N,N'-Diallyl-N,N'-dibenzenesulfonyl-6-bromo-2-methoxy-1,4-phenylenediamine

Base Information

Chemical Name:N,N'-Diallyl-N,N'-dibenzenesulfonyl-6-bromo-2-methoxy-1,4-phenylenediamine
CAS No.:214119-28-5
Molecular Formula:C₂₅H₂₅BrN₂O₅S₂
Molecular Weight:577.52
Hs Code.:

Synonyms:N,N'-Diallyl-N,N'-dibenzenesulfonyl-6-bromo-2-methoxy-1,4-phenylenediamine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N,N'-Diallyl-N,N'-dibenzenesulfonyl-6-bromo-2-methoxy-1,4-phenylenediamine

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Technology Process of N,N'-Diallyl-N,N'-dibenzenesulfonyl-6-bromo-2-methoxy-1,4-phenylenediamine

There total 4 articles about N,N'-Diallyl-N,N'-dibenzenesulfonyl-6-bromo-2-methoxy-1,4-phenylenediamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 106-95-6
allyl bromide

: 214119-26-3
2-bromo-6-methoxy-N¹,N⁴-bis(phenylsulfonyl)-1,4-phenylenediamine

: 214119-28-5
N,N'-Diallyl-N,N'-dibenzenesulfonyl-6-bromo-2-methoxy-1,4-phenylenediamine

Guidance literature:: With tetra-(n-butyl)ammonium iodide; sodium hydride; In tetrahydrofuran; 1.) 50 deg C, 1 h, 2.) reflux, 5 h;
DOI:10.1002/(SICI)1521-3765(19980807)4:8<1554::AID-CHEM1554>3.0.CO;2-J

Reference yield:

: 16618-66-9
2-bromo-6-methoxy-4-nitro-phenylamine

: 214119-28-5
N,N'-Diallyl-N,N'-dibenzenesulfonyl-6-bromo-2-methoxy-1,4-phenylenediamine

Guidance literature:: Multi-step reaction with 3 steps

1: 98 percent / N₂H₄*H₂O, FeCl₃*H₂O, activated carbon / methanol / Heating

2: 81 percent / pyridine / 3 h / 80 °C

3: 80 percent / NaH, nBu₄NI / tetrahydrofuran / 1.) 50 deg C, 1 h, 2.) reflux, 5 h

With pyridine; iron(III) chloride; tetra-(n-butyl)ammonium iodide; sodium hydride; pyrographite; hydrazine hydrate; In tetrahydrofuran; methanol;
DOI:10.1002/(SICI)1521-3765(19980807)4:8<1554::AID-CHEM1554>3.0.CO;2-J

Reference yield:

: 214119-25-2
2-bromo-6-methoxy-1,4-phenylenediamine

: 214119-28-5
N,N'-Diallyl-N,N'-dibenzenesulfonyl-6-bromo-2-methoxy-1,4-phenylenediamine

Guidance literature:: Multi-step reaction with 2 steps

1: 81 percent / pyridine / 3 h / 80 °C

2: 80 percent / NaH, nBu₄NI / tetrahydrofuran / 1.) 50 deg C, 1 h, 2.) reflux, 5 h

With pyridine; tetra-(n-butyl)ammonium iodide; sodium hydride; In tetrahydrofuran;
DOI:10.1002/(SICI)1521-3765(19980807)4:8<1554::AID-CHEM1554>3.0.CO;2-J