1-[5-(2-Chloro-benzyl)-4,5,6,7-tetrahydro-thieno[3,2-c]pyridin-2-yl]-butan-1-one

Base Information

Chemical Name:1-[5-(2-Chloro-benzyl)-4,5,6,7-tetrahydro-thieno[3,2-c]pyridin-2-yl]-butan-1-one
CAS No.:90997-29-8
Molecular Formula:C₁₈H₂₀ClNOS
Molecular Weight:333.882
Hs Code.:

Synonyms:1-[5-(2-Chloro-benzyl)-4,5,6,7-tetrahydro-thieno[3,2-c]pyridin-2-yl]-butan-1-one

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Chemical Property of 1-[5-(2-Chloro-benzyl)-4,5,6,7-tetrahydro-thieno[3,2-c]pyridin-2-yl]-butan-1-one

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Technology Process of 1-[5-(2-Chloro-benzyl)-4,5,6,7-tetrahydro-thieno[3,2-c]pyridin-2-yl]-butan-1-one

There total 1 articles about 1-[5-(2-Chloro-benzyl)-4,5,6,7-tetrahydro-thieno[3,2-c]pyridin-2-yl]-butan-1-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 55142-85-3
ticlopidine

: 141-75-3
butyryl chloride

: 90997-29-8
1-[5-(2-Chloro-benzyl)-4,5,6,7-tetrahydro-thieno[3,2-c]pyridin-2-yl]-butan-1-one

Guidance literature:: With tin(IV) chloride; In dichloromethane; Ambient temperature;

Reference yield: 75.0%

: 90997-29-8
1-[5-(2-Chloro-benzyl)-4,5,6,7-tetrahydro-thieno[3,2-c]pyridin-2-yl]-butan-1-one

: 790615-52-0
2-Butyl-5-(2-chloro-benzyl)-4,5,6,7-tetrahydro-thieno[3,2-c]pyridine

Guidance literature:: With sodium tetrahydroborate; trifluoroacetic acid; In dichloromethane; for 3h; Ambient temperature;

Reference yield:

: 90997-29-8
1-[5-(2-Chloro-benzyl)-4,5,6,7-tetrahydro-thieno[3,2-c]pyridin-2-yl]-butan-1-one

: 90997-45-8
(2-Butyl-thieno[3,2-c]pyridin-3-yl)-(4-methoxy-phenyl)-methanone

Guidance literature:: Multi-step reaction with 5 steps

1: 75 percent / NaBH₄, trifluoroacetic acid / CH₂Cl₂ / 3 h / Ambient temperature

2: 42 percent / SnCl₄ / CH₂Cl₂ / 20 h / Ambient temperature

3: 90 percent / N-bromosuccinimide / CHCl₃ / 3 h / Ambient temperature

4: 82 percent / 10percent Pd/C / ethanol / Heating

5: 31 percent / 1,4-diazabicyclo<2.2.2>octane / dimethylformamide / 6 h / 120 °C

With 1,4-diaza-bicyclo[2.2.2]octane; sodium tetrahydroborate; palladium on activated charcoal; N-Bromosuccinimide; tin(IV) chloride; trifluoroacetic acid; In ethanol; dichloromethane; chloroform; N,N-dimethyl-formamide;