benzyl (11bR)-11b-(4-(N,N-diallylamino)-2,3-dimethoxyphenyl)-8-(methylsulfonyloxy)-1,2,4,5-tetrahydro-6-oxo-4H-indolo[3,2,1-de][1,5]naphthyridine-3(11bH)-carboxylate

Base Information

Chemical Name:benzyl (11bR)-11b-(4-(N,N-diallylamino)-2,3-dimethoxyphenyl)-8-(methylsulfonyloxy)-1,2,4,5-tetrahydro-6-oxo-4H-indolo[3,2,1-de][1,5]naphthyridine-3(11bH)-carboxylate
CAS No.:1196967-88-0
Molecular Formula:C₃₇H₃₉N₃O₈S
Molecular Weight:685.798
Hs Code.:

benzyl (11bR)-11b-(4-(N,N-diallylamino)-2,3-dimethoxyphenyl)-8-(methylsulfonyloxy)-1,2,4,5-tetrahydro-6-oxo-4H-indolo[3,2,1-de][1,5]naphthyridine-3(11bH)-carboxylate

Synonyms:benzyl (11bR)-11b-(4-(N,N-diallylamino)-2,3-dimethoxyphenyl)-8-(methylsulfonyloxy)-1,2,4,5-tetrahydro-6-oxo-4H-indolo[3,2,1-de][1,5]naphthyridine-3(11bH)-carboxylate

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Chemical Property of benzyl (11bR)-11b-(4-(N,N-diallylamino)-2,3-dimethoxyphenyl)-8-(methylsulfonyloxy)-1,2,4,5-tetrahydro-6-oxo-4H-indolo[3,2,1-de][1,5]naphthyridine-3(11bH)-carboxylate

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Technology Process of benzyl (11bR)-11b-(4-(N,N-diallylamino)-2,3-dimethoxyphenyl)-8-(methylsulfonyloxy)-1,2,4,5-tetrahydro-6-oxo-4H-indolo[3,2,1-de][1,5]naphthyridine-3(11bH)-carboxylate

There total 1 articles about benzyl (11bR)-11b-(4-(N,N-diallylamino)-2,3-dimethoxyphenyl)-8-(methylsulfonyloxy)-1,2,4,5-tetrahydro-6-oxo-4H-indolo[3,2,1-de][1,5]naphthyridine-3(11bH)-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1196967-95-9
C₃₇H₄₁N₃O₉S

: 1196967-88-0
benzyl (11bR)-11b-(4-(N,N-diallylamino)-2,3-dimethoxyphenyl)-8-(methylsulfonyloxy)-1,2,4,5-tetrahydro-6-oxo-4H-indolo[3,2,1-de][1,5]naphthyridine-3(11bH)-carboxylate

Guidance literature:: C₃₇H₄₁N₃O₉S; With thionyl chloride; N,N-dimethyl-formamide; In dichloromethane; at 20 ℃; for 0.666667h; Inert atmosphere;

With N-ethyl-N,N-diisopropylamine; at 20 ℃; for 0.583333h; Inert atmosphere;
DOI:10.1002/anie.200902192

Reference yield: 93.0%

: 1196967-88-0
benzyl (11bR)-11b-(4-(N,N-diallylamino)-2,3-dimethoxyphenyl)-8-(methylsulfonyloxy)-1,2,4,5-tetrahydro-6-oxo-4H-indolo[3,2,1-de][1,5]naphthyridine-3(11bH)-carboxylate

: 1196967-89-1
benzyl (11bR)-11b-(4-amino-2,3-dimethoxyphenyl)-8-(methylsulfonyloxy)-1,2,4,5-tetrahydro-6-oxo-4H-indolo[3,2,1-de][1,5]naphthyridine-3(11bH)-carboxylate

Guidance literature:: With tetrakis(triphenylphosphine) palladium⁽⁰⁾; 1,3-dimethylbarbituric acid; In dichloromethane; at 20 ℃; Inert atmosphere; Reflux;
DOI:10.1002/anie.200902192