3-(4-Methoxy-phenyl)-propionic acid (1R,2S)-1-phenethyl-2-trimethylsilanyl-but-3-enyl ester

Base Information

Chemical Name:3-(4-Methoxy-phenyl)-propionic acid (1R,2S)-1-phenethyl-2-trimethylsilanyl-but-3-enyl ester
CAS No.:357914-68-2
Molecular Formula:C₂₅H₃₄O₃Si
Molecular Weight:410.629
Hs Code.:

Synonyms:3-(4-Methoxy-phenyl)-propionic acid (1R,2S)-1-phenethyl-2-trimethylsilanyl-but-3-enyl ester

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3-(4-Methoxy-phenyl)-propionic acid (1R,2S)-1-phenethyl-2-trimethylsilanyl-but-3-enyl ester

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Technology Process of 3-(4-Methoxy-phenyl)-propionic acid (1R,2S)-1-phenethyl-2-trimethylsilanyl-but-3-enyl ester

There total 1 articles about 3-(4-Methoxy-phenyl)-propionic acid (1R,2S)-1-phenethyl-2-trimethylsilanyl-but-3-enyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 15893-42-2
3-(4-methoxyphenyl)propionyl chloride

: (3R,4S)-1-Phenyl-4-trimethylsilanyl-hex-5-en-3-ol

: 357914-68-2
3-(4-Methoxy-phenyl)-propionic acid (1R,2S)-1-phenethyl-2-trimethylsilanyl-but-3-enyl ester

Guidance literature:: With pyridine; dmap; In dichloromethane;
DOI:10.1055/s-2001-14632

Reference yield:

: 357914-68-2
3-(4-Methoxy-phenyl)-propionic acid (1R,2S)-1-phenethyl-2-trimethylsilanyl-but-3-enyl ester

: 3-(4-Methoxy-phenyl)-1-((1R,2S)-1-phenethyl-2-trimethylsilanyl-but-3-enyloxy)-propan-1-ol

Guidance literature:: With diisobutylaluminium hydride; at -78 ℃;
DOI:10.1055/s-2001-14632

Reference yield:

: 357914-68-2
3-(4-Methoxy-phenyl)-propionic acid (1R,2S)-1-phenethyl-2-trimethylsilanyl-but-3-enyl ester

: 357914-69-3
Acetic acid 3-(4-methoxy-phenyl)-1-((1R,2S)-1-phenethyl-2-trimethylsilanyl-but-3-enyloxy)-propyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: DIBAL / -78 °C

2: 79 percent / DMAP; pyridine

With pyridine; dmap; diisobutylaluminium hydride;
DOI:10.1055/s-2001-14632